High accuracy NMR chemical shift corrected for bulk magnetization as a tool for structural elucidation of dilutable microemulsions. Part 1 - Proof of concept
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- 作者：Roy E. Hoffman ; royh63@gmail.com" class="auth_mail" title="E-mail the corresponding author ; Eliezer Darmon Eliezer.darmon@mail.huji.ac.il" class="auth_mail" title="E-mail the corresponding author ; Abraham Aserin abraham.aserin@mail.huji.ac.il" class="auth_mail" title="E-mail the corresponding author ; Nissim Garti garti@mail.huji.ac.il" class="auth_mail" title="E-mail the corresponding author
- 关键词：NMR ; Chemical shift ; Microemulsion ; Analytical chemistry
- 刊名：Journal of Colloid and Interface Science
- 出版年：2016
- 出版时间：1 February 2016
- 年：2016
- 卷：463
- 期：Complete
- 页码：349-357
- 全文大小：1204 K
文摘
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NMR chemical shift is shown to be useful for analyzing microemulsions.
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We measured chemical shift free of bulk magnetization using HR-MAS.
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Mesophase transitions had a noticeable effect on chemical shift.
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This method was validated for a known system.