Determination of 11 quinolones in bovine milk using immunoaffinity stir bar sorptive microextraction and liquid chromatography with fluorescence detection
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- 作者：Kai Yao ; Wei Zhang ; Linyan Yang ; Jianfang Gong ; Liuan Li ; Tianming Jin ; Cun Li ; hhlicun@163.com" class="auth_mail" title="E-mail the corresponding author
- 关键词：Immunoaffinity stir bar ; Quinolone ; Monoclonal antibody ; Bovine milk ; Liquid chromatography
- 刊名：Journal of Chromatography B, Analytical Technologies in the Biomedical and Life Sciences
- 出版年：2015
- 出版时间：15 October 2015
- 年：2015
- 卷：1003
- 期：Complete
- 页码：67-73
- 全文大小：935 K
文摘
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Quantification of 11 QNs in bovine milk.
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Monoclonal antibody to QNs was immobilized to glass bar.
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An immunoaffinity SBSME-LC-FLD method was firstly developed and validated.
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Different conditions during sample preparation were optimized.
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The column capacity and stability of immunoaffinity sitr bar was investigated.