用户名: 密码: 验证码:
P型核磁测井解释处理方法研究
详细信息    本馆镜像全文|  推荐本文 |  |   获取CNKI官网全文
摘要
针对引进的多台Halliburton公司的P型核磁共振成像测井仪,剖析了其特殊的采集模式和数据记录格式,完成了时间域和深度域的P型核磁处理技术研究,提出了一种改善核磁测井油气识别的方法,自行研制了一套符合区域地质条件的核磁测井精细解释处理软件。软件的时间域处理效果与国外公司的解释处理结果完全一致,在参数选取和处理速度等方面更加灵活和方便快捷。
     从第一类积分方程的反演求解入手,讨论了核磁解谱方法,推导出适合于岩石核磁弛豫多指数反演的三种方法(改进的奇异值分解法和模平滑法及联合迭代反演SIRT法),对这些算法的具体实现过程进行了详细的论述,从理论和实例处理两方面讨论分析了三种算法优缺点。讨论了解的分辨率,并给出了最优反演模型的选取原则,奇异值分解算法适合于信噪比较高的核磁弛豫数据反演,模平滑算法灵活性较大,适应于较低信噪比的核磁弛豫数据反演。在解谱的基础上,对P型核磁的T2谱拼接与平滑进行了深入的研究,利用硬拼接和三次样条插值法,对T2谱进行处理,与国外软件的处理结果相比较,取得了良好的效果。
     总结了前人对于岩石孔隙中内流体极化扩散弛豫规律的研究成果,分析了岩石孔隙中内梯度场下油水弛豫规律,在广泛调研国内外核磁共振流体识别方法的基础上,利用T1 T2搜索来识别流体的研究思路,在时间域内搜索计算T1 T2的值,然后进行油气分析,计算各种流体的孔隙度,油气识别技术从定性识别到定量计算变为可能。
It has cost much for China to import some MRIL-P made by Hallliburton, the processing software of which is the processing and analyzing systems based on the geological situation of oil and gas aboard. Therefore there exist some analyzing and processing methods in the systems which are not suitable for the situation of China. On the other hand, the high cost of the imported software and its cost in the processing and interpretation will also increase that of NMR logging. So it is not advisable to spread this kind of logging method in China.
     The thesis deals with the following points:
     First, DPP and PETROSITE by Hallliburton are seriously anatomized. By analyzing its manners of NMR logging, it makes clear of the .cls format to form the foundation of the later data processing.
     It studies on the signal preprocessing method in NMR logging.
     The records in NMR logging are a couple of channels of spin echoes that need a filtering processing and an estimate of the signal phase, so an echo signal curve including the spin echo scope as well as noise, which is used to process the T2 spectrum inversion and so on, and a noise curve only including noise, which is used to analyze the logging quality, can be obtained. Phase correcting, smoothness stacking and filtering processing on NMR logging data is necessary when a signal curve is ensured.
     MRIL-P makes time but not actual logging depth as its index to record the NMR logging signals, so it is necessary to convert the time index to the actual logging depth.
     The NMR curve processed previously is a porosity decay line which can not reflect the porosity situation directly. So it is necessary to invert the decay line into several T2 relaxation time as well as the sizes of the corresponding porosity, that is, to invert into the T2 distribution.
     Second, it analyzes particularly the T2 inversion by the means combining mathematics and physics, and induces three kinds of methods: norm smoothing method and SVD method. It makes a contrastive analysis on the merits and demerits between them theoretically and experimentally. The norm smoothing method is stable and is easy to realize the non-negativity confine, also the result has a reasonable continuity and a high resolution .This method is suitable for the data inversion when SNR is above 20. SVD is fast speed and is reasonable when SNR is above 80. But it can result in the abnormality of T2 spectrum owing to the constraint of non-negativity confine although it suppresses noise excessively. Considering their differences responding to SNR, and taking into account of the relationship among the SVD coordination factorλ, norm smoothing factorαand SNR, the thesis argues that establishing the corresponding method of correction can improve the quality of the inverted results.
     Third, the thesis studies how to confirm the reservoir parameter of NMR porosity on the basis of T2 spectrum inversion. It studies to establish the models of NMR porosity and permeability explanation, and to ascertain the reservoir parameters such as NMR total porosity, NMR effective porosity, clay bound fluid porosity, capillary bound fluid porosity, bound fluid saturation, permeability and so on.
     Taking the logging research in Liaohe region for example, the thesis makes a close study on the NMR features of the reservoir rocks, establishes the NMR analysis parameters ,analysis standard and analysis models fit for the conditions of the reservoir in Liaohe and analyzes the NMR logging data by the self-developed software ,therefore to search some new favorable zones.
     It studies the relationship between the NMR relexation stamp and rock petrophysics property systematically, to clarify the similarities and differences between the logging results of NMR and analysis results of conventional core. It selects kinds of the rock of oil-gas reservoir to research on many aspects such as reservoir fluid NMR properties, NMR T2 response, pore size distribution, porosity, permeability, moveable fluid and T2 cutoff time and the impact of paramagnetic ion on NMR logging and so on.
     The reservoir water salinity and formation temperature have small influence on NMR signal. The signal intensity and value in the condition of high mineralization of water is a little smaller than that of the purified water. So the reservoir water salinity and formation temperature have small impact on the NMR logging results.
     As the NMR spectrum of sandstone core sample is similar to throat radius distribution, it can be converted to pore distribution or capillary pressure- saturation curve. The reduction eoefficient differs in terms of places, and it is often well night the same when in the same core sample reservoir of the same oil field.
     The thesis sums up the former researching findings for the internal flow in the rock pore and analyzes the oil and water relaxation law of G in rock pores. Based on a wide research on how to identify NMR fluid at home and abroad, identifying fluid is conducted by means of T1T2.,and then is converted into T2 spectrum to reduce the influence of noise. So the effect of the different T2 is perfect.
     Finally ,Based on the above research, MRIL-P software in a microcomputer version is developed on the platform of LEAD. When this software is applied to process and analyze the logging data, it leads to a better result compared to that through the DPP.
引文
1.阿克谢利罗德M.著,梅忠武译.核磁测井[M].北京:石油工业出版社,1982 .
    2.查传钰,车文华,顾伟康.用核磁测井资料评价岩石孔径分布[J].江汉石油学院学报,1998,20(2):38-42.
    3.陈福利,张淑品,李冬梅.用核磁T2谱法评价原始气藏流体饱和度——以大庆深层火山岩复杂气藏为例[J].天然气地球科学,2007,18(3):412-417.
    4.付金华.利用核磁测井精细评价低渗透砂岩气层[J].天然气工业,2002,22(6):39-42.
    5.胡俊.NMR评价低阻储集层岩石物性参数研究[J].天然气工业,2002,22(5):42-44.
    6.胡以良,王敬农主编.核磁共振测井译文集[C].潜江:江汉测井研究所,1996.
    7.何宗斌,倪静,伍动等.根据烃与水的T2差异确定含烃饱和度[J].石油天然气学报,2007,29(5): 92-96.
    8.江玉龙,王祝文,伍东.关于提高核磁测井差分谱油气显示方法的研究[J].东华理工大学学报, 2008 , 31(1):59-64.
    9.江玉龙,王祝文,伍东. P型核磁解释处理方法研究[J].吉林大学学报(地球科学版). 2008, 38(3): 208-513.
    10.李天降,李子丰,郭振华等.致密砂岩气藏核磁共振测井与常规测井的孔与渗透模型关系[J].核技术,2007,30(7).
    11.李召成,孙建孟,耿生臣等.应用核磁共振测井T2谱划分裂缝型储层[J].石油物探, 2001, 40(4): 113-118.
    12.刘堂宴,王绍民.核磁共振谱的孔喉结构分析[J].石油地球物理勘探,2003,38(3):328-333.
    13.陆大卫,江国法等编.核磁共振测井理论与应用[J].北京:石油工业出版社,1998年.
    14.宁从前,用双Tw核磁共振测井计算T1直接识别油气层的方法[J].测井技术,2001,25(2):123-126.
    15.马建海,孙建孟,孙萌等.基于迭代Tikhonov正则化的核磁测井解谱方法研究[J].西南石油大学学报,2009,31(1):37-40.
    16.莫修文,李舟波,梅忠武.核磁测井资料的解释方法与应用[J].测井技术,1997,21(6):424-431.
    17.彭石林.顺磁物质对核磁驰豫特性影响的实验研究[J].石油物探,2002,41 (3).
    18.彭石林译.胡以良校.核磁共振测井应用的岩石物理机理[J].测井技术信息,1997,10(4):117-141.
    19.彭石林,胡以良,刘崇汉.岩心核磁共振实验分析与常规物性测量对比[J].测井技术.1998,22(增刊):6-10.
    20.齐宝权,夏宏泉,张贤辉. NMR测井识别储层流体性质的方法及应用[J].西南石油学院学报, 2001, 23(1):18-21.
    21.谭海芳.核磁共振测井在致密气藏评价中的应用[J].测井技术,2007,31(2):144-146.
    22.邵维志,陆福.碳酸盐岩储层流体性质识别新技术[J].测井技术,2002,26(1) :60-63.
    23.邵维志,丁娱娇.MRIL-P型核磁共振测井技术及应用[J].测井技术,2002,26(3):205-212.
    24.谭茂金,石耀霖,赵文杰等核磁共振双TW测井数据联合反演与流体别[J].地球物理学报,2008,51(5):1582-1590.
    25.童茂松,李莉.泥质砂岩的激发极化弛豫时间谱反演[J].测井技术,2005,30(1):64-61.
    26.童茂松,李莉,王伟男等.岩石激发极化弛豫时间谱与孔隙结构、渗透率的关系[J].地球物理学报,2005,48(3):710-716.
    27.王栋,姜在兴等.利用核磁共振测井资料进行烃源岩评价[J].西安石油大学学报(自然科学版), 2004, 19(2):29-32.
    28.王才志,尚卫忠.应用奇异值分解算法的核磁共振测井解谱方法[J].石油地球物理勘探,2003,38(1): 91-94.
    29.王为民.核磁共振测井基础实验研究[J].测井技术,1997,21(6):385-392.
    30.王为民,李培,叶朝辉.核磁共振弛豫信号的多指数反演[J].中国科学(A辑)[J]. 2001,44(11):730-736.
    31.王忠东.核磁共振岩心基础实验分析[J].测井技术,2001,25(3):170-174.
    32.王忠东,汪浩,向天德.综合利用核磁谱差分与谱位移测井提高油层解释精度[J].测井技术,2001, 25(5): 365-368.
    33.汪中浩,章广成,肖承文等.低渗透储层T2截止值实验研究及其测井应用[J].石油物探,2004,45(3): 508-510.
    34.王俊明,邵维志,韩成,常庆喜. MRIL-Prime核磁共振测井仪[J].石油仪器,2002,16(6):18-20.
    35.王光海,李高明.用核磁共振测井确定渗透率的原理和方法分析[J].测井技术,2001,25(2):101-104.
    36.王筱文,肖立志.中国陆相地层核磁共振孔隙度研究[J].中国科学(G),2006,36(4):366-374.
    37.王光海,李高明.用核磁共振测井确定渗透率的原理和方法分析[J].测井技术,2001,25(2): 101- 104.
    38.翁爱华,李舟波等.核磁测井数据弛豫谱反演软件研究[J].长春科技大学学报,2000,31(4): 395- 397.
    39.翁爱华,李舟波,莫修文等.核磁共振测井数据高分辨率反演方法研究[J].测井技术, 2002, 26(6): 455-459.
    40.翁爱华,李舟波,陆敬安,莫修文.高分辨率反演方法及其在核磁共振测井数据处理中的应用[J].石油地球物理勘探,2003,38(2):208-212.
    41.翁爱华.核磁测井数据处理基础理论与实验研究[d].长春:吉林大学博士论文, 2001.
    42.翁爱华,李舟波,王雪秋等.基于回归M-估计的核磁测井数据反演[J].石油地球物理勘探,2002, 37(3):258-261.
    43.肖立志,石红兵.低场核磁共振岩心分析及其在测井解释中的应用[J].测井技术,1998,22(1):42- 49.
    44.肖立志.核磁共振成像测井与岩石核磁共振及其应用[M].北京:科学出版社,1998
    45.肖立志,谢然红.核磁共振在石油测井与地层油气评价中的应用[J].中国工程科学,2003,5(9):87-94.
    46.肖立志,刘堂宴,傅容珊.利用核磁共振测井评价储层的捕集能力[J].石油学报,2004,25(4): 38-41.
    47.肖立志.成像测井学应用基础[M].北京:石油工业出版社,2007.
    48.肖亮,刘晓鹏,毛志强.结合NMR和毛管压力资料计算储层渗透率的方法[J].石油学报,2009,30(1):100-103.
    49.谢然红,肖立志.二维核磁共振测井[J].测井技术,2005,29(5):430-434.
    50.徐立强,何宗斌,郭书生. MRIL_Primer回波信号生成关键技术[J].工程地球物理学报,2008,5(1): 42-48.
    51.岳文正,陶果,赵克超.用核磁共振及岩石物理实验求地层束缚水饱和度及平均孔隙半径[J].测井技术, 2002,26(1):22-25.
    52.姚绪刚,王忠东.一种新的核磁共振弛豫谱反演算法.测井技术,2003,27(5): 23-26.
    53.张莉萍,高勇,杨伟金.核磁共振测井在合川构造低阻油气藏的应用.石油仪器,2008,22(5):65-67.
    54.周灿灿,程相志,司兆伟等.核磁共振自旋回波串确定渗透率方法探讨[J].测井技术,2002, 26(2): 123-126.
    55.朱友青,付有升,杨晓玲.核磁共振测井在深层天然气勘探中的应用[J].测井技术,1998,22(增刊): 77-80.
    56. Akkurt,R.,Mardon,D.,Gardner,j.s,Marshall,D.MandSolanet,F.ENHANCE.diffusion;Expanding the range or NMR direct hydrocarbon typing applications[J], SPWLA, 1998,39th ,Paper.GG.
    57. Akkut,R., prammer,M.G.and Moore,M.A..Selection sr optimal acquisition parameter for MRIL logs[J],The Log Analyst, 1996, 37(6):43-52..
    58. Akkurt,R.,Viegar,H.J., Tutunjian,P.N.,and Guillory,A.J. NMR logging of natural gas reservoirs[J], The Log Analyst, 1996,47(6):33-42.
    59. Akselrod,S.M.,DanerichV.L., Sadikhov, D.M. and Mamed-zadeh,V.A.Downhole lateral nuclear magnetic sounding[J], The Log Analyst, 1996, 37(4): 25-28
    60. Appel,M.,Freem,J.J., Perkins, R.B.and van Dijk,N.P. Reservoir fluid study by nuclear magnetic resonance[J] ,SPWLA, 2000, 41sh ,PAPER:HH.
    61. Baldwin,B.A. and Yamanashi, W.S. NMR imaging of fluid saturation distribution in cores[J], The Log Analyst, 1991, 32(5):536-549.
    62. Banavr,J.R.and Schwart,L.M. Manetic resonance as a probe of permeability in porous media[J],physical Reviws Leters, 1987, 58(14):1411-1414.
    63. Baldwin,B.A., Yamanashi,W.S.Capillary-pressure detemnination from NMR images of centrifuged coue plugs:berea Sandstones[J],The Log Analyst, 32(5):550-556.
    64. Borgia,G.C.,Brigheni, G., Fanzzini,P.,Fanti,G.D.,and Mesini,E..Specific surface and fluid transport in sandstnes throughu NMR studies[J],SPEFE, 1991,7:206-210.
    65. Borgi,G.C.A new unfree fluid index in sandstones through NMR studies[J],SPEFE,1994,9(6):89-93
    66. Borwn,R.J.S. and Fatt,I, Measurement of fractional werrability of oil fields’rochs by the nuclear magnetic relaxation method,: Society of Petroleum Engineer, Richardason, Texas1956,SPE-743-G.
    67. Borwn,R.J.S..Information available and unavailable from multiexponential relaxation data[J],journal of Magnetic Resonance, 1989,82:539.
    68. Brownstein,J.A.and Tarr,C.E..Importance of classical diffusion in NMR studies of water in biological cells[J],Physical Review A, 1979,19(6): 2446-2453.
    69. Buller,D..Carbonate evaluation using NMR time domain analysis[J],SPWLA, 2000, 41th Paper. GGG.
    70. Chang,C.T.,and Edwards,C.M. Proton MR two-component chemical shift imaging of fluids in porous media[J],The Log Analyst, 1993,34(6):20-27
    71. Chang,C.P., Qiao,J., Chen,S., and Wastson.A.T. Invetigating the utility of NMR spectroscopic techniques fou fracture characterization[J], SPWLA, 1996,37th Paper.QQ
    72. ChangD.,Vingegar,H.,Morriss, C.and Straley,C..Effective porosity, producible fulid and permeability in carbonates from NMR Logging[J],The Log Analyst, 1997,38(2): 60-72
    73. Chave,A.D., Thomson,D.J. and Ander,M.E. On the robust estimation of power spectra, coherences, and transfer functions,Journal of Geophysical Research, 1987,92(B1): 633-648.
    74. Chen,S.,Arro,R.,Minetto,C.,Georgi,D.and Liu..C.Methods fou computing SWI and BVI fom NMR logs[J], SPWLA, 1998,39th ,paper:HH.
    75. Christian Straley. Reassessment of Correlations of between Viscosity and NMR Measurement[J], SPWLA, 47th ,2006,Paper:AA.
    76. Claerbout,J.F.and Muir,F. Robust modeling with drratic data[J], Geophysics, 1973,38(5):826 -844
    77. Calloges,D.P.,Muun,K.,Smith,D.M.,and Stermer,D.L..A NMR technique for the analysis of pore structure: Application to materials with well-defined pore structure[J],Joumal of Colloid and Interface Science, 1987,119(1):127-140.
    78. Coates,G.R.,Demoo,S..The producibility answer product[J], Slumberger technical review, 1988,25(2): 55-63.
    79. Coates,G.R.,,Marschall,D.,.Mardon,D.,and Galford,J..A new characterization of bulk- volume irreducible using magnetic resonance[J],SPWLA, 38th ,1997,Paper.QQ.
    80. Coates,G.R..,Miller,D.L.,Mardon,D.,and Gardner,J.S..Applying log measurements lf restricted diffusion and T2 to formation evaluation[J], SPWLA, 36th ,1995,Paper.p.
    81. Cohen,M.H. and Mendelson,K.S..Nuclear magnetic relaxation and the internal geometry of sedimentary rocks[J],J.App.Phys., 1982,53(2):1127-1135.
    82. Crampin, Tom . Well log facies classification for improved regional exploration [J].Exploration Geophysics (Melbourne), 2008vol. 39, no. 2:115-123.
    83. Curwen,D.W., Molaro,C..Permeability from magnetic resonance imaging Logs[J], SPWLA, 36th ,1995,Paper.GG.
    84. Decoster, Eric.Application of recent NMR developments to the characterization of Orinoco Belt heavy oil reservoirs[J].Petrophysics (Houston, Tex.), 2008 ,vol. 49, no. 2:191-192.
    85. Dodge,W.S., Shafer, J.L.,and Angel,G.G..Core and Log NMR measurements of an iron-rich, glaucontic sandstone reservoir[J],SPWLA, 36 th ,1995, Paper:O.
    86. Dodge,W.S., Shafer,J.L.,and Klimentidis,R.E., Capillary pressure:the key to producible porosity[J], SPWLA, 37th ,1996,Paper3..
    87. Dunn,K-J.,Bergman,D.J., LaTorraca,G.A., Stonare,S.M., and Growe,,.B..A method for inverting NMR data sets with different signal to noise ratios,SPWLA, 39th ,1998,Paper.JJ
    88. Dunn,K-J.Bergman and G.A.LaTorraca.Nuclear Magnetic Resonance Petrophysical and Logging Aplications[M]. New York :Pergamon,2002.
    89. Egbert,G. D., and Bookerr,J.R..Robust detimation sf geomagnetic transfer functions[J], Geophys . J.R.,astr.soc., 1986, 38(5): 826-844.
    90. Edwards,C.M. andChen,S.. Improved NMR well logs from time-dependent echo filtering [J]SPWLA, 37th 1996,Paper:RR.
    91. Eidesmo,T.,Relling,O.M.,and Rueslatten,H..NMR. Logging sf mixed-wet north sea sandstone reservoirs[J],SPWLA, 37th ,1996,Paper:PP .
    92. Flaum,C.,Guru,L., and Banerjee,S.. Saturation estimation from magnetic in carbonates[J], SPWLA, 37th 2000,Paper:HHH.
    93. Flaum,C.,Kjenberg,R.L., and Hurliman,M.D.. Identification sf gas with the combinable magnetic resonance tool {CMR}[J],SPWLA, 37th ,1996,Paper:L.
    94. FLOlo,L.H., Getting the hydrocarbon volumes right—a quantitative use of NMR data in water saturation modeling[J],SPWLA, 39th ,1998,Paper:Y
    95. Freedman,R.,Minh,C.C.Gubelin,Gubelin,G.,Freeman,J.J.,McGinness,T.,Terry.,B.,and Rawlence, D.. Combining NMR and density logs for petrophysical analysis in gas-bearing formations[J], SPWLA, 39th ,1998,Paper:ll.
    96. Gallegos,D.P.,and.Smith,D.M., A.NMRtechnique for the analysis of pore structure: detemnination of continuous pore size distributions,Joumal of Colloid and interface [J],Science, 1988,122: 186-198.
    97. Gonzalez-Perez, Martha.C NMR and FTIR spectroscopy characterization of humic acids in Spodosols under tropical rain forest in southeastern Brazil[J]. Geoderma, 2008 vol. 146, no. 3-4:425-433.
    98. Gossenbirg,p.,Galli,G..Andreani,M.,and Klopf,W., A new petrophysical interpretation moodel for classicao rocks based on NMR, epithemmal neutron and electromagnetic logs[J] , SPWLA, 37th , 1996, Paper.M.
    99. Hamada, Gharib M.New NMR approach evaluates tight gas sand reservoirs.Oil & Gas Journal,2008, vol. 106, no. 21:46-53.
    100. Hook,J.R., Basan,P.B.,and lovwden,B.D..The MRIL Log in a low Porosity formation[J], SPWLA, 37th , 1996,Paper:N.
    101. Heaton,N.n Minh,C.C.,Freedman,R,and Flaum,C.. High-resolution bound-fluid,free-fluid and porosity with fast NMR Logging[J],SPWLA, 41st , 2000,Paper:V.
    102. Horkowitz,J.P., Vinegar,H.J., Hartman,D.E.,Coates,G.R., and Clerke,E.A..Residual oil saturation measurements in carbonates wih pulsed NMR Logs[J],SPWLA, 36th ,1995,Paper:Q.
    103. Howard,J.J.. Wettability and fluid saturation determined from NMR TI distribution[J],Magnetic Resonance Imaging, 1994,12(2):197-200.
    104. Howard J.J., and Spiner,E.A..Nuclear magnetic resonance measurements of wettability and fluid saturions in chalk[J], SPE , 1994,26471.
    105. Hussein,S.M.,Hassan,S.,Klimentos,T.,Boy,A., Usiing NMR and electrical Logs for enhanced evaluation of producibility and hydrocarbon reservoirs with high irreducible water saturation[J],SPWLA, 40th ,1999,Paper:HH.
    106. Keller, Margaret A.Petroleum source-rock potential of late Paleocene and early Eocene wilcox and Claiborne Group strata determined by geophysical well-log analysis: Zapata County[J], Texas.Abstracts with Programs Geological Society of America, 2008 ,vol. 40, no.6:305.
    107. Kenyon,W.E..Petrophysical properties of application of NMR LoggingV, the Analyst, 1997,38(2): 21-43.
    108. Kleinberg,R.L.,and Vinegar,H.J..NMR.,prperties of reservoir fluids[J],The Log Analyst, 1996, 37(6): 20-32.
    109. Kroeker,R.M.,and Henkelman,R,M..Analysis of biological NMR relaxation data with continrous distributions of relaxation times,Joumal of Magnetic Resonnace, 1986,69:218-235.
    110. Kumar,A.T..Measurement of aperture and multiphase flow in fractures using NMR imaging[J],SPE, 1996,30558.
    111. LaTorraca,G.A.,Stonard,S.W.,Webber.P.R.,Carlson,R.M.,andDunn,K.J..Heavy oil viscosity detemmination using NMRlogs[J],SPWLA, 40th ,1999,Paper:PPP.
    112. Lee,SB.,Kim,L,C.,Millet,C.A.and Torquato,S.. Random-walk simulation of diffusion- controlled processes among static traps[J],Physical Review B, 1989,39(16): 11833-11839.
    113. Looyestijn, W.J..Determination of oil saturation from diffusion NMR logs[J],SPWLA, 37th ,1996,Paper:SS.
    114. Mason, Harris E, McCubbin, Francis M,Smirnov, Alexander,Phillips, Brian L . Solid-state NMR and IR spectroscopic investigation of the role of structural water and F in carbonate-rich fluorapatite[J], American Mineralogist,2009 , vol. 94, no. 4, pp.507-516,
    115. McKen,D.,Minh,C.C.,Freedman,R.,Harris,R.,Willis,D.,Dauies,D.,Gubelin,Gubelin,G.,Oldigs,R. and Hurlimann,M., Percolation model of nuclear magnetic relaxation in porous media[J], Physical Review B, 1990,41(1): 562-567.
    116. Menge,S.And Pranmer,M..Can NMR porosity replace comventional porosity in formation evaluation? [J],SPWLA, 39th ,1998,Paper:RR .
    117. Mirta,P.P.,and Sen,P,N., Effects of microneometry and surface relaxation on NMR pulsed-fiele-Gradient experiments:Simple pore geomtries[J],Physical Review B, 1992, 45(1): 143- 156
    118. Mitra,P,P.,Sen,P.N., and Schwartz,L.M., Short-time behavior of diffusion coefficient as ageometrical probe of porous media,Phsical Review B, 1993,47(14): 8565-8574.
    119. Morriss,C.E.,Deutch,P.,Freedman,R.,McKen,D.,AndKleinberg,R.L..Operating guide for the combinable magnetic resonance tool[J],The Log Analyst, 1996,37(6): 53-60.
    120. Morris,C.E.,Maclnnis,J.,Freedman,r.Smaardyk,J..STRALEY, Field test of an experimental pulsed nuclear magnetism tool,paper FFF,in 34th annual logging symposium transactions :Society of Professinonal Well Log Analysts[J], 1993,23p.
    121. Morrisss,C.E.,Freedman,R.,Straley,C.,Jonhson,M.,Kenyon,W.E., Vinegar,H,J., and Tutunjian, P.N.. Hydrocarbon saturation and viscosity estimation from NMR,logging in the belridae diatomite[J],The Log Analyst, 1997, 38(2): 44-49.
    122. Morriss,C.E.,Msclnnis,R.,Freedman, R.,Smaardyk.R.J.. Field ttest of an experimental pulsed nuclear magnetism tool[J], SPWLA., 34th ,1993,Paper.GGG.
    123. Munn,K.,and Smith,D.M..A NMR technique for the analysis of pore struchre:Numerical inversion of relaxation measurements[J],Journal of Colloid and Interface Science, 1987, 119(1):117-126.
    124. NAAascimento,D.S., and Denicol,P.S.. Reduction lf the effect from NMR toolmotion on the estimation lf bound water[J],SPWLA, 40th ,1999,Paper:11.
    125. Nelson,P.H..Permeability-porosity relationships in sedimentary rocks[J],The Log Analyst, 1994, 35(3): 38-61.
    126. Ostroff,G.M., Sjpreu,P.S., and Geogri,D.T.. Integration of NMR and conventional log data for improved petrophysical evaluation of shaly sands[J],SPWLA, 40th ,1999,Paper.OOO.
    127. Petricola,M.K., and Troussant,X.. Application s of fast NMR logging in shaly gas-bearing sands invaded by oil filtrate[J]SPWLA, 40th ,1999,Paper:QQQ.
    128. Prammer,M.G., Mardon,D., Coates, G.R., and Miller,M.N., Lithology-independent gas detection by gradient-NMR logging[J], SPE, 1995,30562
    129. Prammer,M.G.,Bouton,J., Chandler,R.N.,and Drack,E.D..A new multiband generation of NMR logging tools[J], SPWLA, 40th ,1999,Paper:DD.
    130. Prammer,M.G.,Drack,E.D.,Bouton,J.C.and Gardner,J.S.. Measurements of clay-bound water and total porosity by magnetic resonance logging[J],The log Analyst, 1996,47(6):61-69.
    131. Prammer,M.G., Goodman,G.D., Menger,S.K., Morys,M., and Zannoni.S..Field test of an experimental NMRLWD device[J],SPWLA, 41st ,2000,Paper:EEE.
    132. Prammer,M.G., NMR pore size distributions and permeability at the well site[J],SPE,1994.28368
    133. Ramakrishnan,T.S., Scjwartz,;.M., Fordham,E.J., Kenyon, W.E., and Wilkinson, D.J..Forward models for nuclear magnetic resonance in carbonate rocks[J],SPWLA, 39th ,1998,Paper:SS..
    134. Ramakrishnan,T.S., Fordham,E.J.,Venkataramanan,L., Flaum,M., and Schwartz,L.M..new interpretation methodology based on forward models fro magnetic resonance in carbonates, [J]SPWLA, 40th ,1999,Paper:MMM..
    135. Ray, Satyaki.Concepts of facies geocellular modeling in oilsands using image log and dipmeter data within the Krishna Godavari Delta basin[J]. Reservoir,2008 vol. 35, no. 8:16.
    136. Sakurai,S., Loucks,R.G., and Gardner, J.S.,.NMR core analysis of lower San Andres/Cloieta/Upper Clear Fork {Permian}carbonates:Central Basin Platform,West Texas[J],SPWLA, 36th ,1995, Paper:M.
    137. Schmidt,E.J., Velasco,K.K.,and Nur,A.M..Puantifying solid-fluid interfacial phenomena in porous rocks with proton nuclear magnetic resonance[J],journal of Applied Physics, 1986,59(8): 2788-2797.
    138. Seevers,D.O..A nuclear magnetic method for determining the permeability of sandstones[J], SPWLA, 7th 1966,Paper:L.
    139. Slikerman,W.F.J.,et al.Society of Petroleum Engineers,Houston[J],SPE,1999, Paper 56768.
    140. Sen,P.N., Schwartz,L.M., Mitra,P.P.,and Halperin,B.I., Surface relaxation and the long-tim diffusion coefficient in porous media:Periodic geometry[J],Physical Review B., 1994,49(1): 215-225
    141. Sen,P.N.,Straley,C.,Kenyon,W.E.andWhittingham,M.S..Surface-to-Volume ratio, charge density, nuclear magnetic relaxation,and permeability in clay-bearing sandstones[J], Geophysics, 1990,55(1):61-69.
    142. Sezginer,A., Minh,C.C., Heaton,N., Freedman,R., and Dort,G.V..An NMR hing-resolution permeability indicatou[J],SPWLA, 40th ,1999,Paper:NNN.
    143. Straley,C. Rossini,D., Vinegar,H., Tutunjian,P.And Morriss,C..Core analysis by low-field NMR[J], The Log A nalyst, 1997, 38(2): 84-95.
    144. Straley,C., Morriss,c.e., Kenyon,W.E., and Howard,J.J..NMR in partially saturated rocks: Laboratory insights on free fluid index and comparison with borehole logs[J],The Log Analyst, 1995,36(1): 40-56.
    145. Sun B, Dunn K-J, Bilodeau B J,Van Dalen S C.Stonard SW and Al-Rushaid M A. Two-dimensional NMR Logging and Field Test Results[J]. SPWLA, 45th ,2000, Paper:KK.
    146. Tabry,J.,Fleury,M., Locatelli,M.,and Martin,J,P., A high resolutioNMR logging tool:concept validation[J], SPWLA, 41th ,2000, Paper:Z.
    147. Tang,X.M., Altunbay,M., and Shoey,D., Joint interpretation of formation permeability from wireline acoustic, NMR and Image log data[J],SPWLA, 39th ,1998,Paper:KK..
    148. Them,H.F.,Mardon,D.Lorsong,J.A.,Cen,S.,Dodge,S.AndOstroff,G., Time-domain correction of MRIL log contaminated by borehole signal[J],SPWLA, 41st ,2000,Paper:Y.
    149. Timur,A..An investigation of permeability, porosity and residual water saturation relationships[J],SPWLA9th ,1968,Paper:K.
    150. Timur,A..A Producible porosity and permeability of sandstones investigated through nuclear magnetic resonance principles[J],The Log A nalyst, 1969 9(1): 3-11.
    151. Timur,A.. Pusled nuclear magnetic resonance studies of porosity ,movable f luid,and permeability of sandstones[J],SPE,1969,2045.
    152. Timur,A.. Nuclear magnetic resonance study of carbonate rocks[J],The Log Analyst, 1972,3(5): 3-11.
    153. Torquato,S., Kim,I.C..Effectint simulation technique to compute effective properties of heterogeneous media[J],Appl.phys.Lett., 1989,55:1847-1849.
    154. Volokitin,Y.,Looyestijn,W., Slijkerman W.,and Hofman,J.. Constructing capillary pressure curves from NMR log data in the pressing o hydrocarbons [J], PWLA 40th , 1999, aper: K K K.
    155. White, Jim.Continuous characterization of multiple fluids in a North Sea gas condensate reservoir by integrating downhole NMR with downhole sampling[J]. Petrophysics (Houston, Tex.),2008,vol. 49, no. 2:213.
    156. Whitall,K.P.,and Mackey,A.L..Quantitative interpretation of NMR relaxation data[J],Journal of Magnetic Resonance, 1989, 84:134-152.
    157. Wilkinson,D.J. Johnson,D.L..and Schwrtz,L.M., Nulear magnetic relaxation in porous media The role of the mean life time T {P,D}[J],Physical Review B, 1991, 44(10):4960-4972.
    158. Yamashita, Shigeru.Water speciation in sodium silicate glasses based on NIR and NMR spectroscopy[J] .Chemical Geology, vol. 256, no. 3-4, pp.231-241.
    159. Zhang,Q.,Lo., So-W., Huang.C.C., Hirasaki,G.J., Kobayashi,R. and House,W.V., Some exceptions to default NMR rock and fluid properties[J],SPWLA, 39th ,1998,Paper:FF.
    160. Zheng,L., Chiew,Y.C.. Computer simulation of diffusion-controlled reactions in dispersions of apherical sinks, [J]J.Chem.Phys, 1989,90(1):322-327.

© 2004-2018 中国地质图书馆版权所有 京ICP备05064691号 京公网安备11010802017129号

地址:北京市海淀区学院路29号 邮编:100083

电话:办公室:(+86 10)66554848;文献借阅、咨询服务、科技查新:66554700