单颗粒电化学:纳米颗粒及生物分子的分析检测（英文）
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摘要
单颗粒碰撞电化学近年来已得到迅速发展并在纳米颗粒的性质分析及包括DNA、RNA、蛋白质、酶、细菌、病毒、囊泡类物质等生物体的检测上展示出广阔的前景.在这篇综述中,作者总结了近年来单颗粒碰撞电化学在电化学分析中的进展,按分析检测的策略不同分为以下几个部分阐述:纳米粒子或标记纳米粒子的直接电解;包含氧化还原活性分子的软颗粒的直接电解;颗粒的间接电化学行为;区域扩散阻塞效应;电流强度及碰撞频率的改变.
Single particle impact electrochemistry(SPIEC) has grown rapidly in recent years and shown great promise in the analysis of nanoparticle properties as well as the detection of biomolecules including DNA, RNA, protein, enzyme, bacteria, virus,vesicles and others. This minireview summarizes recent advances in electroanalytical applications of SPIEC according to different analytical methods, i.e., direct electrolysis of nanoparticles or labeled nanoparticles, direct electrolysis of soft particles encapsulated redox molecule, indirect electrochemistry of particles, area and diffusion blocking, and changes in current magnitude and collision frequency.
Single particle impact electrochemistry(SPIEC) has grown rapidly in recent years and shown great promise in the analysis of nanoparticle properties as well as the detection of biomolecules including DNA, RNA, protein, enzyme, bacteria, virus,vesicles and others. This minireview summarizes recent advances in electroanalytical applications of SPIEC according to different analytical methods, i.e., direct electrolysis of nanoparticles or labeled nanoparticles, direct electrolysis of soft particles encapsulated redox molecule, indirect electrochemistry of particles, area and diffusion blocking, and changes in current magnitude and collision frequency.
引文
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[22]Sokolov S V,Tschulik K,Batchelor-McAuley C,et al.Reversible or not?Distinguishing agglomeration and aggregation at the nanoscale[J].Analytical Chemistry,2015,87(19):10033-10039.
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[25]Chen L F,Tanner E E L,Lin C H,et al.Impact electrochemistry reveals that graphene nanoplatelets catalyse the oxidation of dopamine via adsorption[J].Chemical Science,2018,9(1):152-159.
[26]Xiang Z P,Deng H Q,Peljo P,et al.Electrochemical dynamics of a single platinum nanoparticle collision event for the hydrogen evolution reaction[J].Angewandte Chemie International Edition,57(13):3464-3468.
[27]Tschulik K,Haddou B,Omanovic D,et al.Coulometric sizing of nanoparticles:cathodic and anodic impact experiments open two independent routes to electrochemical sizing of Fe3O4nanoparticles[J].Nano Research,2013,6(11):836-841.
[28]Zampardi G,Thoming J,Naatz H,et al.Electrochemical behavior of single CuO nanoparticles:implications for the assessment of their environmental fate[J].Small,2018,14(32):1801765.
[29]Zhao L J,Qian R C,Ma W,et al.Electrocatalytic efficiency analysis of catechol molecules for NADH oxidation during nanoparticle collision[J].Analytical Chemistry,2016,88(17):8375-8379.
[30]Zhou Y G,Rees N V,Compton R G.The electrochemical detection of tagged nanoparticles via particle-electrode collisions:nanoelectroanalysis beyond immobilisation[J].Chemical Communications,2012,48(19):2510-2512.
[31]Cheng W,Zhou X F,Compton R G.Electrochemical sizing of organic nanoparticles[J].Angewandte Chemie International Edition,2013,52(49):12980-12982.
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[33]Kim B K,Kim J,Bard A J.Electrochemistry of a single'attoliter emulsion droplet in collisions[J].Journal of the American Chemical Society,2015,137(6):2343-2349.
[34]Feng A,Cheng W,Compton R G.Measuring the oxygen content of a single oil droplet[J].Chemical Science,2016,7(10):6458-6462.
[35]Lebègue E,Anderson C M,Dick J E,et al.Electrochemical detection of single phospholipid vesicle collisions at a Pt ultramicroelectrode[J].Langmuir,2015,31(42):11734-11739.
[36]Dunevall J,Fathali H,Najafinobar N,et al.Characterizing the catecholamine content of single mammalian vesicles by collision-adsorption events at an electrode[J].Journal of the American Chemical Society,2015,137(13):4344-4346.
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[38]Cheng W,Compton R G.Investigation of single-drug-encapsulating liposomes using the nano-impact method[J].Angewandte Chemie International Edition,2014,53(50):13928-13930.
[39]Cheng W,Compton R G.Measuring the content of a single liposome through electrocatalytic nanoimpact“titrations”[J].ChemElectroChem,2016,3(12):2017-2020.
[40]Kwon S J,Bard A J.DNA analysis by application of Pt nanoparticle electrochemical amplification with single label response[J].Journal of the American Chemical Society,2012,134(26):10777-10779.
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