Surface adhesive properties of continuous PBO fiber after air-plasma-grafting-epoxy treatment

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• 作者：Cai-xia Jia 贾彩霞 ; Qian Wang 王乾 ; Ping Chen 陈平…
• 关键词：Key wordsplasma grafting ; continuous PBO fiber ; surface adhesive properties ; heat resistance
• 刊名：Journal of Central South University
• 出版年：2016
• 出版时间：September 2016
• 年：2016
• 卷：23
• 期：9
• 页码：2165-2172
• 全文大小：1,750 KB
• 刊物类别：Engineering
• 刊物主题：Engineering, general
  Metallic Materials
  Chinese Library of Science
  
• 出版者：Central South University, co-published with Springer
• ISSN：2227-5223
• 卷排序：23

文摘

It was found that air dielectric barrier discharge (DBD) plasma contributed to the grafting of epoxy resin onto continuous PBO fiber surface. This air-plasma-grafting-epoxy method yielded a noticeable enhancement in the interfacial adhesion between PBO fiber and thermoplastic matrix resin, with the interlaminar shear strength of the resulting composites increased by 66.7%. DSC and FTIR analyses were then used to study the curing behavior of epoxy coating on PBO fiber surface, deduce the possible grafting reactions and investigate the grafting mechanism. More importantly, TGA measurement showed that the grafting of epoxy onto PBO fiber had almost no effect on the composite heat resistance, and there was more thermoplastic matrix resin adhering to the fiber surface; the latter could also be clearly found in the SEM photos. Thereby, the air-plasma-grafting-epoxy treatment was proved to be an effective method for the improvement of continuous PBO fiber surface adhesive properties.