- 中文主题词：分光光度法 ; 铁 ; 分析 ; 钴 ; 试验 ; 铜 ; 锌 ; 银 ; 镍 ; 铅 ; 金属 ; 丁二酮肟 ; 铊 ; 镍含量 ; 锰 ; 锡 ; 碲 ; 合金 ; 镉 ; 碳含量 ; 氮 ; 硒 ; 铋 ; 砷 ; 氧 ; 原子吸收 ; 导热性
- 标准号：ASTM E1587-2005
- 发布日期：2005
- 英文题名：Standard Test Methods for Chemical Analysis of Refined Nickel
- 英文主题词：bismuth ; cadmium ; cobalt ; copper ; flame atomic absorption ; iron ; lead ; manganese ; refined nickel ; silver ; spectrometry ; zinc ; antimony ; arsenic ; bismuth ; cadmium ; electrothermal atomic absorption spectrometry ; lead ; refined nickel ; selenium ; silver ; tellurium ; thallium ; tin ; hydrogen sulfide ; methylene blue ; refined nickel ; spectrophotometry ; sulfur
- 标准状态：现行
- 发布单位：US-ASTM
- 国际标准分类号：77.120.40 (Nickel, chromium and their alloys)
- 载体形态：12P.;A4
- 中国标准分类号：H13
- 国别：美国材料与试验协会
These test methods are primarily intended to test refined nickel metal for compliance with compositional specifications. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that the analytical work will be performed in a properly equipped laboratory under appropriate quality control practices.
1.1 These test methods apply to the chemical analysis of refined nickel and other forms of metallic nickel having chemical compositions within the following limits:
| Element | Weight % |
| Antimony, less than | 0.005 |
| Arsenic, less than | 0.005 |
| Bismuth, less than | 0.01 |
| Cadmium, less than | 0.0025 |
| Carbon, max | 0.03 |
| Cobalt, max | 1.00 |
| Copper, max | 1.00 |
| Hydrogen, max | 0.003 |
| Iron, max | 0.15 |
| Lead, less than | 0.01 |
| Manganese, less than | 0.20 |
| Nickel, min | 98.0 |
| Nitrogen, less than | 0.50 |
| Oxygen, less than | 0.03 |
| Phosphorus, less than | 0.005 |
| Selenium, less than | 0.0010 |
| Silicon, less than | 0.005 |
| Silver, less than | 0.01 |
| Sulfur, max | 0.01 |
| Tellurium, less than | 0.0010 |
| Thallium, less than | 0.0010 |
| Tin, less than | 0.005 |
| Zinc, less than | 0.015 |
1.2 These test methods may be used to determine the following elements by the methods indicated below:
| Antimony, Arsenic, Bismuth, Cadmium, Lead, Selenium, Silver, Tellurium, Tin, and Thallium by the Electrothermal Atomic Absorption Method |
| Bismuth, Cadmium, Cobalt, Copper, Iron, Lead, Manganese, Silver, and Zinc by the Flame Atomic Absorption Method |
| Carbon, Total, by the Combustion-Instrumental Method |
| Nickel by the Dimethylglyoxime Gravimetric Method |
| Nitrogen by the Inert Gas Fusion Thermal Conductivity Method |
| Oxygen by the Inert Gas Fusion Method |
| Sulfur by the Infrared Absorption Method |
| Sulfur by the Methylene Blue Spectrophotometric Method After Generation of Hydrogen Sulfide |
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precautions, see Section 6.
© 2004-2018 中国地质图书馆版权所有 京ICP备05064691号 京公网安备11010802017129号 地址：北京市海淀区学院路29号 邮编：100083 电话：办公室：(+86 10)66554848；文献借阅、咨询服务、科技查新：66554700 |