ATR红外光谱分析在贝诺酯合成实验中的应用
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摘要
以贝诺酯的合成实验为例,介绍了ATR红外光谱分析在有机合成实验教学实践中的应用,学生通过该实验,学会了如何应用ATR红外光谱这一常规分析手段解决合成中实际遇到的问题,科研思维能力明显提高。同时,通过对滤液中原料的回收,节约了教学成本,培养学生养成良好的科研习惯和环保意识。
Takes the synthesis of benorilate as an example, this paper introduces the application of ATR-IR in the teaching practice of organic synthesis experiment, through this experiment, students have learned how to use ATR-IR as a conventional analytical method to solve the practical problems encountered in synthesis, and their scientific research thinking ability has been greatly improved. At the same time, through the recycling of raw materials in filtrate, the teaching cost is saved, and students are trained to form good scientific research habits and environmental awareness.
Takes the synthesis of benorilate as an example, this paper introduces the application of ATR-IR in the teaching practice of organic synthesis experiment, through this experiment, students have learned how to use ATR-IR as a conventional analytical method to solve the practical problems encountered in synthesis, and their scientific research thinking ability has been greatly improved. At the same time, through the recycling of raw materials in filtrate, the teaching cost is saved, and students are trained to form good scientific research habits and environmental awareness.
引文
[1] 吴瑾光.近代傅立叶变换红外光谱技术及应用[ M].北京:科学技术文献出版社,1994.
[2] 孟长功,辛剑.基础化学实验[M].2版.北京:高等教育出版社,2009.
[3] 刘芙,陈立新,王艳华,等.高校大型仪器平台面向实验教学开放的思考与研究[J].中国现代教育装备,2018(3):4-5,8.
[4] 朱顺平,薛英.ATR的工作原理、校准及检测[J].北京测绘,2005(3):26-29.
[5] 刘咏,倪春明,李斌.红外ATR技术在液体样品检验中的应用研究[J].云南警官学院学报,2017(4):101-105.
[6] 徐琳,王乃岩,王云龙,等.傅里叶变换衰减全反射红外光谱的应用与进展[J].光谱学与光谱分析,2004,24(3):317-319.
[7] 黄红英,尹齐和.傅里叶变换衰减全反射红外光谱法(ATR-FTIR)的原理与应用进展[J].中山大学研究生学刊(自然科学、医学版),2011,32(1):20-31.
[8] 彭司勋.药物化学[M].北京:中国医药科技出版社,1999:117.
[9] 刘改枝,薛令平,贾永艳,等.贝诺酯的合成工艺综述与对比分析[J].河南科学,2018,36( 9) :1362 -1366.
[10] 王莹.贝诺酯的合成及表征[J].实验科学与技术,2014,12(4):32-34.
[2] 孟长功,辛剑.基础化学实验[M].2版.北京:高等教育出版社,2009.
[3] 刘芙,陈立新,王艳华,等.高校大型仪器平台面向实验教学开放的思考与研究[J].中国现代教育装备,2018(3):4-5,8.
[4] 朱顺平,薛英.ATR的工作原理、校准及检测[J].北京测绘,2005(3):26-29.
[5] 刘咏,倪春明,李斌.红外ATR技术在液体样品检验中的应用研究[J].云南警官学院学报,2017(4):101-105.
[6] 徐琳,王乃岩,王云龙,等.傅里叶变换衰减全反射红外光谱的应用与进展[J].光谱学与光谱分析,2004,24(3):317-319.
[7] 黄红英,尹齐和.傅里叶变换衰减全反射红外光谱法(ATR-FTIR)的原理与应用进展[J].中山大学研究生学刊(自然科学、医学版),2011,32(1):20-31.
[8] 彭司勋.药物化学[M].北京:中国医药科技出版社,1999:117.
[9] 刘改枝,薛令平,贾永艳,等.贝诺酯的合成工艺综述与对比分析[J].河南科学,2018,36( 9) :1362 -1366.
[10] 王莹.贝诺酯的合成及表征[J].实验科学与技术,2014,12(4):32-34.