魔芋中活性成分联产工艺研究
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- 英文论文题名：Study on Joint Producing Technology of Active Ingredients from Konjac
- 论文作者：周秀秀 ; 徐乐乐 ; 叶晶 ; 靳素荣
- 英文论文作者：Xiuxiu Zhou ; Lele Xu ; Jing Ye ; Surong Jin ; Chemistry and Life Sciences ; Wuhan University of Technology
- 年：2016
- 作者机构：武汉理工大学化学化工与生命科学学院化学系;
- 论文关键词：联产工艺 ; 魔芋 ; 葡甘聚糖 ; 生物碱 ; 神经酰胺
- 英文论文关键词：Joint Producing Technology ; Konjac ; Konjac Glucomannan ; Alkaloids ; Ceramides
- 会议召开时间：2016-07-01
- 会议录名称：中国化学会第30届学术年会摘要集-第二十三分会：复杂样品分离分析
- 语种：中文
- 分类号：TQ914.1
- 学会代码：ZGHY
- 会议名称：中国化学会第30届学术年会-第二十三分会 ; 复杂样品分离分析
- 会议地点：中国辽宁大连
- 主办单位：中国化学会
- 学会名称：中国化学会
- 页数：1
- 文件大小：143k
- 原文格式：D
- 会议级别：全国
摘要
以魔芋为研究对象,采用超声辅助联产工艺法对其活性成分进行研究。用正交优化试验考察了提取神经酰胺与生物碱的影响因素,确定了最佳提取工艺条件:提取温度为60℃、乙醇浓度为70%、提取时间为20min、料液比为1:40。在此条件下得到魔芋中神经酰胺提取率为1.57mg/g,生物碱提取率为0.41mg/g。采用柱层析、重结晶等技术纯化后神经酰胺和生物碱的纯度分别为80.77%和71.68%;采用乙醇沉淀法从魔芋残渣中提取KGM类化合物,提取率为0.51g/g,纯化后的纯度为93.86%。本研究对提高魔芋的综合利用,降低生产成本,增加附加经济值,提高经济效益具有重要意义。
With Konjac as the research object,the active components were studied by ultrasonic assisted co-production technology.The factors affecting the extraction of ceramide and alkaloids were investigated by orthogonal test,and the optimum extraction conditions were determined as follows:temperature 60℃,70%ethanol,time 20 min,liquid material ratio 1:40.After being separatedand purified,the ceramide was 1.57mg/g,purity was 80.77%;the alkaloid was 0.41mg/g,purity was 71.68%;the extraction rate of KGM was 0.51g/g by ethanol precipitation method,and the purity was 93.86%.Studing on the joint producing technology of the acive ingredients from Konjac plays very significant meaning for raising comprehensive use,decreasing production cost,increasing economical values and benefits.
With Konjac as the research object,the active components were studied by ultrasonic assisted co-production technology.The factors affecting the extraction of ceramide and alkaloids were investigated by orthogonal test,and the optimum extraction conditions were determined as follows:temperature 60℃,70%ethanol,time 20 min,liquid material ratio 1:40.After being separatedand purified,the ceramide was 1.57mg/g,purity was 80.77%;the alkaloid was 0.41mg/g,purity was 71.68%;the extraction rate of KGM was 0.51g/g by ethanol precipitation method,and the purity was 93.86%.Studing on the joint producing technology of the acive ingredients from Konjac plays very significant meaning for raising comprehensive use,decreasing production cost,increasing economical values and benefits.
引文
[1]Tao Fan,Optimization of enzymolysis-ultrasonic assisted extraction of polysaccharides from Momordica charabtia L.by response surface methodology[J],2015,115(09):701-706
[2]Xuegang Luo,The mechanism of sodium hydroxide solution promoting the gelation of Konjac glucomannan(KGM)[J],Food Hydrocolloids,2013,30(10):92-99
[2]Xuegang Luo,The mechanism of sodium hydroxide solution promoting the gelation of Konjac glucomannan(KGM)[J],Food Hydrocolloids,2013,30(10):92-99