高真空精馏技术在单体香料提纯领域的应用研究
详细信息 查看官网全文
- 英文论文题名：Application investigation of high vacuum distillation technology used in the Purification of monomers spices
- 论文作者：许保云 ; 翟金国 ; 艾波 ; 王传昌
- 英文论文作者：Xu Bao-yun ; Zhai Jin-guo ; Ai Bo ; Wang Chuan-chang ; Shanghai research institute of chemical industry
- 年：2016
- 作者机构：上海化工研究院;
- 论文关键词：高真空 ; 间歇精馏 ; 单体香料 ; 分离提纯
- 英文论文关键词：high vacuum distillation ; batch distillation ; monomers spices ; separation and purification
- 会议召开时间：2016-06-15
- 会议录名称：第十一届中国香料香精学术研讨会论文集
- 英文会议录名称：The Proceedings of the 11th Seminar on Fragrance and Flavor China
- 语种：中文
- 分类号：TQ651
- 学会代码：ZGXE
- 会议名称：第十一届中国香料香精学术研讨会
- 会议地点：中国上海
- 主办单位：中国香料香精化妆品工业协会
- 学会名称：中国香料香精化妆品工业协会
- 页数：4
- 文件大小：259k
- 原文格式：O
- 会议级别：全国
摘要
本文对高真空间歇精馏技术进行总结,介绍了其技术特点,认为该技术适用于热敏性、高沸点物质的分离提纯,可作为香精香料的分离手段被广泛应用。本文结合几个单体香料分离的实际案例,证实了高真空间歇精馏技术用于分离提纯单体香料的实用性。
The high vacuum batch distillation technology is summarized in this paper and its technical feature is introduced.Because of the advantage of applying to the separation of heat-sensitive constituents and high-boiling point substance,it can be widely used as the separation process in the essence and flavor industry.The industrial applicability of the high vacuum batch distillation technology used in the monomers spices separation and purification is confirmed by several projects.
The high vacuum batch distillation technology is summarized in this paper and its technical feature is introduced.Because of the advantage of applying to the separation of heat-sensitive constituents and high-boiling point substance,it can be widely used as the separation process in the essence and flavor industry.The industrial applicability of the high vacuum batch distillation technology used in the monomers spices separation and purification is confirmed by several projects.
引文
[1]陈祖霖,邹德正,李飘英.间歇精馏过程动态特性及优化操作研究[J].广西大学学报:自然科学版,1990(2):19-24.
[2]王浩平,项曙光.间歇精馏过程模拟优化研究进展[J].计算机仿真,2004,21(2):4-6.
[3]Christensen F M,Jrgensen S B.Optimal control of binary batch distillation with recycled waste cut[J].Chemical Engineeringjournal,1987,34(2):57-64.
[4]Gonzalezvelasco J R,Gutierrezortiz M A,Castresanapelayo J M,et al.Improvements in batch distillation startup[J].Industrial&Engineering Chemistry Research,2002,26(4):745-750.
[5]白鹏,张卫江,余国琼.动态累积分批精馏过程研究(I)——操作方法及实验[J].化学工程,1994(6):15-18.
[6]Boyd T.Safrit+and,Westerberg A W.Improved Operational Policies for Batch Extractive Distillation Columns[J].Industrial&Engineering Chemistry Research,1997,36(2):436-443.
[7]Sorensen E.A cyclic operating policy for batch distillation-theory and practice[J].Computers&Chemical Engineering,1999,23(s 4-5):533-542.
[8]Lopes M M,Song T W.Batch distillation:Better at constant or variable reflux?[J].Chemical Engineering&Processing,2010,49(12):1298-1304.
[9]C.Zavala,C.Coronado.Optimal Control Problem in Batch Distillation Using Thermodynamic Efficiency[J].Ind.eng.chem.res,2008,47(8):2788-2793.
[10]唐善宏,伍昭化,刘乃鸿,等.精细化工高真空连续精馏技术[C]//2008年全国精馏技术交流与展示大会.2008.
[11]裘炳毅.化妆品化学与工艺技术大全(上下)[M].中国轻工业,2006.
[12]许松林,应安国,王淑华.桃醛的提纯研究[J].香料香精化妆品,2004(5):1-3.
[13]吴立成,许俊英,王复琴,等.合成桃醛香料[J].河北化工,1987(2).
[14]许松林,应安国,王淑华.真空精馏提纯桃醛的研究[J].化工进展,2004,23(6):43-45.
[15]丁宝维,许松林,林涛,等.桃醛的外消旋物的分离研究进展[J].香料香精化妆品,2009(1):37-39.
[16]丁宝维.桃醛合成工艺优化及其动力学研究[D].天津大学,2009.
[17]许松林,应安国,王淑华.桃醛提纯的真空间歇精馏工艺[J].化学工业与工程,2005,22(2):112-114.
[18]张富捐,王经亚,张翔宇.γ-十一内酯的合成研究[J].许昌学院学报,2005,24(2):121-123.
[19]秦榛.γ-十一内酯合成过程特征及反应动力学研究[D].华东理工大学,2014.
[20]梅建凤,陈虹.生物转化法生产β-苯乙醇[J].微生物学通报,2005,32(2):114-118.
[21]赵修报,唐育岐,刘天明.β-苯乙醇的研究进展[J].中国酿造,2011(8):1-4.
[22]Etschmann M,Bluemke W,Sell D,et al.Biotechnological production of 2-phenylethanol.[J].Applied Microbiology&Biotechnology,2002,59(1):1-8.
[23]杨霄,崔志峰.酵母生物转化生产2-苯乙醇的研究进展[J].应用与环境生物学报,2006,12(1):140-144.
[24]Yang X A,Cui Z.Progress in 2-phenylethanol Production by Biotransformation with Yeast[J].Chinese Journal of Applied&Environmental Biology,2006.
[25]Etschmann M M W,Dieter S,Jens S.Production of2-phenylethanol and 2-phenylethylacetate from L-phenylalanine by coupling whole-cell biocatalysis with organophilic pervaporation.[J].Biotechnology&Bioengineering,2005,92(5):624-634.
[26]孙志强,徐杰.β-苯乙醇的制备方法[J].中国科学院大连化学物理研究所,2004.
[27]孙青,舒学军,陈茹冰,等.香料紫罗兰酮的合成研究[J].浙江大学学报:理学版,2012,39(1).
[28]程劼,谢建春,孙宝国.超临界CO2流体色谱分离α-紫罗兰酮和β-紫罗兰酮[J].食品与发酵工业,2008,34(10):10-12.
[29]袁联群,董瑾,孟建良,等.从生产β-紫罗兰酮的精镏副产物中分离回收β-紫罗兰酮[J].上海应用技术学院学报:自然科学版,2004,4(4):290-293.
[2]王浩平,项曙光.间歇精馏过程模拟优化研究进展[J].计算机仿真,2004,21(2):4-6.
[3]Christensen F M,Jrgensen S B.Optimal control of binary batch distillation with recycled waste cut[J].Chemical Engineeringjournal,1987,34(2):57-64.
[4]Gonzalezvelasco J R,Gutierrezortiz M A,Castresanapelayo J M,et al.Improvements in batch distillation startup[J].Industrial&Engineering Chemistry Research,2002,26(4):745-750.
[5]白鹏,张卫江,余国琼.动态累积分批精馏过程研究(I)——操作方法及实验[J].化学工程,1994(6):15-18.
[6]Boyd T.Safrit+and,Westerberg A W.Improved Operational Policies for Batch Extractive Distillation Columns[J].Industrial&Engineering Chemistry Research,1997,36(2):436-443.
[7]Sorensen E.A cyclic operating policy for batch distillation-theory and practice[J].Computers&Chemical Engineering,1999,23(s 4-5):533-542.
[8]Lopes M M,Song T W.Batch distillation:Better at constant or variable reflux?[J].Chemical Engineering&Processing,2010,49(12):1298-1304.
[9]C.Zavala,C.Coronado.Optimal Control Problem in Batch Distillation Using Thermodynamic Efficiency[J].Ind.eng.chem.res,2008,47(8):2788-2793.
[10]唐善宏,伍昭化,刘乃鸿,等.精细化工高真空连续精馏技术[C]//2008年全国精馏技术交流与展示大会.2008.
[11]裘炳毅.化妆品化学与工艺技术大全(上下)[M].中国轻工业,2006.
[12]许松林,应安国,王淑华.桃醛的提纯研究[J].香料香精化妆品,2004(5):1-3.
[13]吴立成,许俊英,王复琴,等.合成桃醛香料[J].河北化工,1987(2).
[14]许松林,应安国,王淑华.真空精馏提纯桃醛的研究[J].化工进展,2004,23(6):43-45.
[15]丁宝维,许松林,林涛,等.桃醛的外消旋物的分离研究进展[J].香料香精化妆品,2009(1):37-39.
[16]丁宝维.桃醛合成工艺优化及其动力学研究[D].天津大学,2009.
[17]许松林,应安国,王淑华.桃醛提纯的真空间歇精馏工艺[J].化学工业与工程,2005,22(2):112-114.
[18]张富捐,王经亚,张翔宇.γ-十一内酯的合成研究[J].许昌学院学报,2005,24(2):121-123.
[19]秦榛.γ-十一内酯合成过程特征及反应动力学研究[D].华东理工大学,2014.
[20]梅建凤,陈虹.生物转化法生产β-苯乙醇[J].微生物学通报,2005,32(2):114-118.
[21]赵修报,唐育岐,刘天明.β-苯乙醇的研究进展[J].中国酿造,2011(8):1-4.
[22]Etschmann M,Bluemke W,Sell D,et al.Biotechnological production of 2-phenylethanol.[J].Applied Microbiology&Biotechnology,2002,59(1):1-8.
[23]杨霄,崔志峰.酵母生物转化生产2-苯乙醇的研究进展[J].应用与环境生物学报,2006,12(1):140-144.
[24]Yang X A,Cui Z.Progress in 2-phenylethanol Production by Biotransformation with Yeast[J].Chinese Journal of Applied&Environmental Biology,2006.
[25]Etschmann M M W,Dieter S,Jens S.Production of2-phenylethanol and 2-phenylethylacetate from L-phenylalanine by coupling whole-cell biocatalysis with organophilic pervaporation.[J].Biotechnology&Bioengineering,2005,92(5):624-634.
[26]孙志强,徐杰.β-苯乙醇的制备方法[J].中国科学院大连化学物理研究所,2004.
[27]孙青,舒学军,陈茹冰,等.香料紫罗兰酮的合成研究[J].浙江大学学报:理学版,2012,39(1).
[28]程劼,谢建春,孙宝国.超临界CO2流体色谱分离α-紫罗兰酮和β-紫罗兰酮[J].食品与发酵工业,2008,34(10):10-12.
[29]袁联群,董瑾,孟建良,等.从生产β-紫罗兰酮的精镏副产物中分离回收β-紫罗兰酮[J].上海应用技术学院学报:自然科学版,2004,4(4):290-293.