Fluorescence Retention of Organosilane-polymerized Carbon Dots Inverse Opals in CuCl Suspension
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摘要
A novel and fluorescence retention inverse opal has been achieved from organosilane-polymerized carbon dots(SiCDs), which is prepared via infiltrating SiCD solution into the interstice of photonic crystal(PC) template, low temperature treatment, heating polymerization and removing the colloidal template. The as-prepared SiCD inverse opals demonstrate close-cell structure, which is completely different from conventional open-cell structure. Then the fluorescence signal of as-prepared sample keeps almost unchanged in CuCl suspension while the fluorescence of SiCD solution can be quenched by CuCl suspension through an effective electron transfer process. This phenomenon can be attributed to the combined effect of high hydrostatic pressure in the pore structure, stable crosslinking network and fluorescence enhancement by PC structure. The SiCD inverse opals have advantages of unique close-cell structure, easy preparation and good repeatability that give an important insight into the design and manufacture of novel and advanced optical devices.
A novel and fluorescence retention inverse opal has been achieved from organosilane-polymerized carbon dots(SiCDs), which is prepared via infiltrating SiCD solution into the interstice of photonic crystal(PC) template, low temperature treatment, heating polymerization and removing the colloidal template. The as-prepared SiCD inverse opals demonstrate close-cell structure, which is completely different from conventional open-cell structure. Then the fluorescence signal of as-prepared sample keeps almost unchanged in CuCl suspension while the fluorescence of SiCD solution can be quenched by CuCl suspension through an effective electron transfer process. This phenomenon can be attributed to the combined effect of high hydrostatic pressure in the pore structure, stable crosslinking network and fluorescence enhancement by PC structure. The SiCD inverse opals have advantages of unique close-cell structure, easy preparation and good repeatability that give an important insight into the design and manufacture of novel and advanced optical devices.
A novel and fluorescence retention inverse opal has been achieved from organosilane-polymerized carbon dots(SiCDs), which is prepared via infiltrating SiCD solution into the interstice of photonic crystal(PC) template, low temperature treatment, heating polymerization and removing the colloidal template. The as-prepared SiCD inverse opals demonstrate close-cell structure, which is completely different from conventional open-cell structure. Then the fluorescence signal of as-prepared sample keeps almost unchanged in CuCl suspension while the fluorescence of SiCD solution can be quenched by CuCl suspension through an effective electron transfer process. This phenomenon can be attributed to the combined effect of high hydrostatic pressure in the pore structure, stable crosslinking network and fluorescence enhancement by PC structure. The SiCD inverse opals have advantages of unique close-cell structure, easy preparation and good repeatability that give an important insight into the design and manufacture of novel and advanced optical devices.
引文
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8 Xu,Y.;Chen,X.;Chai,R.;Xing,C.F.;Li,H.R.;Yin,X.B.A magnetic/fluorometric bimodal sensor based on a carbon dots-Mn O2 platform for glutathione detection.Nanoscale 2016,8,13414-13421.
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25 Rahul,T.K.;Sandhyarani,N.Nitrogen-fluorine co-doped titania inverse opals for enhanced solar light driven photocatalysis.Nanoscale 2015,7,18259-18270.
26 Wang,H.;Gu,H.C.;Chen,Z.Y.;Shang,L.R.;Zhao,Z.;Gu,Z.Z.;Zhao,Y.J.Enzymatic inverse opal hydrogel particles for biocatalyst.ACS Appl.Mater.Interfaces 2017,9(15),12914-12918.
27 Gao,N.;Tian,T.;Cui,J.C.;Zhang,W.L.;Yin,X.P.;Wang,S.Q.;Ji,J.W.;Li,G.T.Efficient construction of well-defined multicompartment porous systems in a modular and chemically orthogonal fashion.Angew.Chem.Int.Ed.2017,56,3880-3885.
28 Zhao,Z.;Wang,H.;Shang,L.R.;Yu,Y.R.;Fu,F.F.;Zhao,Y.J.;Gu,Z.Z.Bioinspired heterogeneous structural color stripes from capillaries.Adv.Mater.2017,29,1704569.
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30 Fu,F.F.;Chen,Z.Y.;Zhao,Z.;Wang,H.;Shang,L.R.;Gu,Z.Z.;Zhao,Y.J.Bio-inspired self-healing structural color hydrogel.Proc.Natl.Acad.Sci.2017,114,5900-5905.
31 Guo,D.;Li,C.;Wang,Y.;Li,Y.N.;Song,Y.L.Precise assembly of particles for zigzag or linear patterns.Angew.Chem.Int.Ed.2017,129,15550-15554.
32 Hou,J.;Li,M.Z.;Song,Y.L.Patterned colloidal photonic crystals.Angew.Chem.Int.Ed.2018,57(10),2544-2553.
33 Xing,H.H.;Li,J.;Shi,Y.;Guo,J.B.;Wei,J.Thermally driven photonic actuator based on silica opal photonic crystal with liquid crystal elastomer.ACS Appl.Mater.Interfaces 2016,8(14),9440-9445.
34 Wei,W.Y.;Shi,A.S.;Wu,T.H.;Wei,J.;Guo,J.B.Thermo-responsive shape and optical memories of photonic composite films enabled by glassy liquid crystalline polymer networks.Soft Matter 2016,12,8534-8541.
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36 Zhou,J.M.;Han,P.;Liu,M.J.;Zhou,H.Y.;Zhang,Y.X.;Jiang,J.K.;Liu,P.;Wei,Y.;Song,Y.L.;Yao,X.Self-healable organogel nanocomposite with angle-independent structural colors.Angew.Chem.Int.Ed.2017,129,10598-10602.
37 Liu,J.C.;Shang,Y.Y.;Zhang,D.J.;Xie,Z.;Hu,R.X.;Wang,J.X.Single-material solvent-sensitive fluorescent actuator from carbon dots inverse opals based on gradient dewetting.Chinese J.Polym.Sci.2017,35(9),1043-1050.
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41 Cheng,J.;Wang,C.F.;Zhang,Y.;Yang,S.Y.;Chen,S.Zinc ion-doped carbon dots with strong yellow photoluminescence.RSC Adv.2016,6,37189-37194.
42 Fan,Y.O.;Cheng,H.H.;Zhou,C.;Xie,X.J.;Liu,Y.;Dai,L.M.;Zhang,J.;Qu,L.T.Honeycomb architecture of carbon quantum dots:a new efficient substrate to support gold for stronger SERS.Nanoscale 2012,4,1776-1781.
43 Eftekhari,E.;Wang,W.T.;Li,X.;Nikhil,A.;Wu,Z.Q.;Klein,R.;Cole,I.S.;Li,Q.Picomolar reversible Hg(II)solid-state sensor based on carbon dots in double heterostructure colloidal photonic crystals.Sensor Actuat.B-Chem.2017,240,204-211.
44 Zhang,W.J.;Zhang,X.Z.;Zhang,Z.X.;Wang,W.H.;Xie,A.J.;Xiao,C.H.;Zhang,H.;Shen,Y.H.A nitrogen-doped carbon dot-sensitized Ti O2 inverse opal film:preparation,enhanced photoelectrochemical and photocatalytic performance.J.Electrochem.Soc.2015,162,H638-H644.
45 Wang,F.;Xie,Z.;Zhang,H.;Liu,C.Y.;Zhang,Y.G.Highly luminescent organosilane-functionalized carbon dots.Adv.Funct.Mater.2011,21,1027-1031.
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2 Wang,L.;Wang,Y.L.;Xu,T.;Liao,H.B.;Yao,C.B.;Liu,Y.;Li,Z.;Chen,Z.W.;Pan,D.Y.;Sun,L.T.;Wu,M.H.Gram-scale synthesis of single-crystalline graphene quantum dots with superior optical properties.Nat.Commun.2014,5,5357.
3 Mahesh,S.;Lekshmi,C.L.;Renuka,K.D.;Joseph,K.Simple and cost-effective synthesis of fluorescent graphene quantum dots from honey:application as stable security ink and white-light emission.Part.Part.Syst.Charact.2016,33,70-74.
4 Zhang,F.;Feng,X.T.;Zhang,Y.;Yan,L.P.;Yang,Y.Z.;Liu,X.J.Photoluminescent carbon quantum dots as a directly film-forming phosphor towards white LEDs.Nanoscale 2016,8,8618-8612.
5 Zhu,L.L.;Yin,Y.J.;Wang,C.F.;Chen,S.Plant leaf-derived fluorescent carbon dots for sensing,patterning and coding.J.Mater.Chem.C 2013,1,4925-4932.
6 Liu,S.S.;Wang,C.F.;Li,C.X.;Wang,J.;Mao,L.H.;Chen,S.Hair-derived carbon dots toward versatile multidimensional fluorescent materials.J.Mater.Chem.C 2014,2,6477-6483.
7 Liu,S.;Tian,J.Q.;Wang,L.;Zhang,Y.W.;Qin,X.Y.;Luo,Y.L.;Asiri,A.M.;Al-Youbi,A.O.;Sun,X.P.Hydrothermal treatment of grass:a low-cost,green route to nitrogen-doped,carbon-rich,photoluminescent polymer nanodots as an effective fluorescent sensing platform for label-free detection of Cu(II)ions.Adv.Mater.2012,24,2037-2041.
8 Xu,Y.;Chen,X.;Chai,R.;Xing,C.F.;Li,H.R.;Yin,X.B.A magnetic/fluorometric bimodal sensor based on a carbon dots-Mn O2 platform for glutathione detection.Nanoscale 2016,8,13414-13421.
9 Miao,X.;Qu,D.;Yang,D.X.;Nie,B.;Zhao,Y.K.;Fan,H.Y.;Sun,Z.C.Synthesis of carbon dots with multiple color emission by controlled graphitization and surface functionalization.Adv.Mater.2018,30,1704740.
10 Liu,J.J.;Lu,S.Y.;Tang,Q.L.;Zhang,K.;Yu,W.X.;Sun,H.C.;Yang,B.One-step hydrothermal synthesis of photoluminescent carbon nanodots with selective antibacterial activity against porphyromonas gingivalis.Nanoscale 2017,9,7135-7142.
11 Lu,S.Y.;Xiao,G.J.;Sui,L.Z.;Feng,T.L.;Yong,X.;Zhu,S.J.;Li,B.J.;Liu,Z.Y.;Zou,B.;Jin,M.X.;Tse,J.S.;Yan,H.;Yang,B.Piezochromic carbon dots with two-photon fluorescence.Angew.Chem.Int.Ed.2017,129,6283-6287.
12 Liu,X.J.;Liu,L.T.;Hu,X.J.;Zhou,S.Y.;Ankri,R.;Fixler,D.;Xie,Z.Multimodal bioimaging based on gold nanorod and carbon dot nanohybrids as a novel tool for atherosclerosis detection.Nano Res.2017,DOI:10.1007/s12274-017-1739-4
13 Xie,Z.;Wang,F.;Liu,C.Y.Organic-inorganic hybrid functional carbon dot gel glasses.Adv.Mater.2012,24,1716-1721.
14 Huang,J.J.;Zhong,Z.F.;Rong,M.Z.;Zhou,X.;Chen,X.D.;Zhang,M.Q.An easy approach of preparing strongly luminescent carbon dots and their polymer based composites for enhancing solar cell efficiency.Carbon 2014,70,190-198.
15 Lu,W.B.;Qin,X.Y.;Liu,S.;Chang,G.H.;Zhang,Y.W.;Luo,Y.L.;Asiri,A.M.;Al-Youbi,A.O.;Sun,X.P.Economical,green synthesis of fluorescent carbon nanoparticles and their use as probes for sensitive and selective detection of Mercury(II)ions.Anal.Chem.2012,84(12),5351-5357.
16 Zheng,M.;Xie,Z.G.;Qu,D.;Li,D.;Du,P.;Jing,X.P.;Sun,Z.C.On-off-on fluorescent carbon dot nanosensor for recognition of Chromium(VI)and ascorbic acid based on the inner filter effect.ACS Appl.Mater.Interfaces 2013,5,1078-1083.
17 Dong,Y.Q.;Wang,R.X.;Li,G.L.;Chen,C.Q.;Chi,Y.W.;Chen,G.N.Polyamine-functionalized carbon quantum dots as fluorescent probes for selective and sensitive detection of copper ions.Anal.Chem.2012,84,6620-6624.
18 Lu,W.J.;Gong,X.J.;Nan,M.;Liu,Y.;Shuang,S.M.;Dong,C.Comparative study for N and S doped carbon dots:synthesis,characterization and applications for Fe3+probe and cellular imaging.Anal.Chim.Acta 2015,898,116-127.
19 Luo,W.;Yan,J.D.;Tan,Y.L.;Ma,H.R.;Guan,J.G.Rotating1 -D magnetic photonic crystal balls with a tunable lattice constant.Nanoscale 2017,9,9548-9555.
20 Wu,Y.N.;Li,F.T.;Zhu,W.;Cui,J.C.;Tao,C.A.;Lin,C.X.;Hannam,P.M.;Li,G.T.Metal-organic frameworks with a three-dimensional ordered macroporous structure:dynamic photonic materials.Angew.Chem.Int.Ed.2011,50,12518-12522.
21 Liu,J.C.;Wan,L.;Zhang,M.B.;Jiang,K.J.;Song,K.;Wang,J.X.;Ikeda,T.;Jiang,L.Electrowetting-induced morphological evolution of metal-organic inverse opals toward a water-lithography approach.Adv.Funct.Mater.2017,27,1605221.
22 Chen,K.;Fu,Q.Q.;Ye,S.Y.;Ge,J.P.Multicolor printing using electric-field-responsive and photocurable photonic crystals.Adv.Funct.Mater.2017,27,1702825.
23 Pang,F.;Jiang,Y.T.;Zhang,Y.Q.;He,M.Y.;Ge,J.P.Synergetic enhancement of photocatalytic activity with a photonic crystal film as a catalyst support.J.Mater.Chem.A2015,3,21439-21443.
24 Waterhouse,G.I.N.;Wahab,A.K.;Al-Oufi,M.;Jovic,V.;Anjum,D.H.;Sun-Waterhouse D.;Liorca,J.;Idriss,H.Hydrogen production by tuning the photonic band gap with the electronic band gap of Ti O2.Sci.Rep.2013,3,2849.
25 Rahul,T.K.;Sandhyarani,N.Nitrogen-fluorine co-doped titania inverse opals for enhanced solar light driven photocatalysis.Nanoscale 2015,7,18259-18270.
26 Wang,H.;Gu,H.C.;Chen,Z.Y.;Shang,L.R.;Zhao,Z.;Gu,Z.Z.;Zhao,Y.J.Enzymatic inverse opal hydrogel particles for biocatalyst.ACS Appl.Mater.Interfaces 2017,9(15),12914-12918.
27 Gao,N.;Tian,T.;Cui,J.C.;Zhang,W.L.;Yin,X.P.;Wang,S.Q.;Ji,J.W.;Li,G.T.Efficient construction of well-defined multicompartment porous systems in a modular and chemically orthogonal fashion.Angew.Chem.Int.Ed.2017,56,3880-3885.
28 Zhao,Z.;Wang,H.;Shang,L.R.;Yu,Y.R.;Fu,F.F.;Zhao,Y.J.;Gu,Z.Z.Bioinspired heterogeneous structural color stripes from capillaries.Adv.Mater.2017,29,1704569.
29 Liu,J.C.;Xie,Z.;Shang,Y.Y.;Ren,J.K.;Hu,R.X.;Guan,B.;Wang,J.X.;Ikeda,T.;Jiang,L.Lyophilic but nonwettable organosilane-polymerized carbon dots inverse opals with close-cell structure.ACS Appl.Mater.Interfaces 2018,10,6701-6710.
30 Fu,F.F.;Chen,Z.Y.;Zhao,Z.;Wang,H.;Shang,L.R.;Gu,Z.Z.;Zhao,Y.J.Bio-inspired self-healing structural color hydrogel.Proc.Natl.Acad.Sci.2017,114,5900-5905.
31 Guo,D.;Li,C.;Wang,Y.;Li,Y.N.;Song,Y.L.Precise assembly of particles for zigzag or linear patterns.Angew.Chem.Int.Ed.2017,129,15550-15554.
32 Hou,J.;Li,M.Z.;Song,Y.L.Patterned colloidal photonic crystals.Angew.Chem.Int.Ed.2018,57(10),2544-2553.
33 Xing,H.H.;Li,J.;Shi,Y.;Guo,J.B.;Wei,J.Thermally driven photonic actuator based on silica opal photonic crystal with liquid crystal elastomer.ACS Appl.Mater.Interfaces 2016,8(14),9440-9445.
34 Wei,W.Y.;Shi,A.S.;Wu,T.H.;Wei,J.;Guo,J.B.Thermo-responsive shape and optical memories of photonic composite films enabled by glassy liquid crystalline polymer networks.Soft Matter 2016,12,8534-8541.
35 Zhou,J.M.;Yang,J.;Gu,Z.D.;Zhang,G.F.;Wei,Y.;Yao,X.;Song,Y.L.;Jiang,L.Controllable fabrication of noniridescent microshaped photonic crystal assemblies by dynamic three-phase contact line behaviors on superhydrophobic substrates.ACS Appl.Mater.Interfaces 2015,7(40),22644-22651.
36 Zhou,J.M.;Han,P.;Liu,M.J.;Zhou,H.Y.;Zhang,Y.X.;Jiang,J.K.;Liu,P.;Wei,Y.;Song,Y.L.;Yao,X.Self-healable organogel nanocomposite with angle-independent structural colors.Angew.Chem.Int.Ed.2017,129,10598-10602.
37 Liu,J.C.;Shang,Y.Y.;Zhang,D.J.;Xie,Z.;Hu,R.X.;Wang,J.X.Single-material solvent-sensitive fluorescent actuator from carbon dots inverse opals based on gradient dewetting.Chinese J.Polym.Sci.2017,35(9),1043-1050.
38 Yablonovitch,E.Inhibited spontaneous emission in solid-state physics and electronics.Phys.Rev.Lett.1987,58,2059-2062.
39 John,S.Strong localization of photons in certain disordered dielectric superlattices.Phys.Rev.Lett.1987,58,2486-2489.
40 Sun,Y.;Zhang,Z.X.;Xie,A.J.;Xiao,C.H.;Li,S.K.;Huang,F.Z.;Shen,Y.H.An ordered and porous N-doped carbon dot-sensitized Bi2O3 inverse opal with enhanced photoelectrochemical performance and photocatalytic activity.Nanoscale 2015,7,13974-13980.
41 Cheng,J.;Wang,C.F.;Zhang,Y.;Yang,S.Y.;Chen,S.Zinc ion-doped carbon dots with strong yellow photoluminescence.RSC Adv.2016,6,37189-37194.
42 Fan,Y.O.;Cheng,H.H.;Zhou,C.;Xie,X.J.;Liu,Y.;Dai,L.M.;Zhang,J.;Qu,L.T.Honeycomb architecture of carbon quantum dots:a new efficient substrate to support gold for stronger SERS.Nanoscale 2012,4,1776-1781.
43 Eftekhari,E.;Wang,W.T.;Li,X.;Nikhil,A.;Wu,Z.Q.;Klein,R.;Cole,I.S.;Li,Q.Picomolar reversible Hg(II)solid-state sensor based on carbon dots in double heterostructure colloidal photonic crystals.Sensor Actuat.B-Chem.2017,240,204-211.
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