用户名: 密码: 验证码:
多氯酚的样品前处理及分析检测研究
详细信息    查看全文 | 推荐本文 |
  • 英文篇名:Advances on Sample Pretreatment and Analysis of Multi Chlorophenols
  • 作者:刘育坚 ; 杨玉明 ; 许志刚
  • 英文作者:LIU Yu-jian;YANG Yu-ming;XU Zhi-gang;Faculty of Science,Kunming University of Science and Technology;
  • 关键词:多氯酚 ; 样品前处理 ; 分析检测
  • 英文关键词:multi chlorophenols;;sample pretreatment;;analysis
  • 中文刊名:HXSS
  • 英文刊名:Chemical World
  • 机构:昆明理工大学理学院;
  • 出版日期:2016-12-22 09:03
  • 出版单位:化学世界
  • 年:2017
  • 期:v.58
  • 基金:国家自然科学基金(No.21565018);; 昆明理工大学大学生创新(Nos.201610674055,2015BA124)资助项目
  • 语种:中文;
  • 页:HXSS201704011
  • 页数:9
  • CN:04
  • ISSN:31-1274/TQ
  • 分类号:53-61
摘要
多氯酚是一类毒性高并具有致癌性的污染物,由于其使用广泛,环境中残留的多氯酚类化合物对人体造成的危害日益得到重视,对环境中的多氯酚类化合物进行评估、分析和检测十分重要。综述了多氯酚化合物的样品前处理方法,包括固相萃取、固相微萃取、液相微萃取、膜萃取、分子印迹聚合物微萃取、搅拌棒吸附萃取和微波辅助萃取等,并对常用的检测技术进行了介绍,包括高效液相色谱法、气相色谱法、液质联用法、气质联用法和毛细管电泳法等。
        Multi chlorophenol is a class of highly toxic and carcinogenic pollutants,and it is widely used in our daily life.The harms to humans caused by multi chlorophenol residues in environment have got more and more attention.It is important to evaluate,analyze and detect multi chlorophenol in environment.The sample pretreatment methods of multi chlorophenol were summarized,including solid phase extraction,solid phase microextraction,liquid phase microextraction,membrane separation,molecularly imprinted polymer microextraction,stir bar sorptive extraction and microwave assisted extraction.The common detection techniques were also introduced,including high performance liquid chromatography,gas chromatography,liquid chromatography-mass spectrometry,gas chromatography-mass spectrometry and capillary electrophoresis.
引文
[1]蒋洁,陈江宁,于红霞,等.多氯酚类化合物对离体培养细胞的QSAR研究及毒性机理初探[J].科学通报,2004,49(2):125-129.
    [2]周丽新.陈晓红,金朱聪.氯酚的分析技术研究进展[J].卫生研究,2014,43(4):685-692.
    [3]王彦丽.多氯酚污染物的降解研究进展[J].安徽农业科学,2009,37(30):14 858-14 861.
    [4]李攻科,胡玉玲,阮贵华.样品前处理仪器与装置[M].北京:化学工业出版社,2007:1-4.
    [5]张海霞,朱彭龄.固相萃取[J].分析化学,2000,28(9):1 172-1 180.
    [6]HASSINE S B,HAMMAMI B,TOUIL S,et al.Determination of Chlorophenols in Water Samples Using Solid-phase Extraction Enrichment Procedure and Gas Chromatography Analysis[J].Bull Environ Contam Toxicol,2015,95(5):654-660.
    [7]石莹,张晶,卢丽彬,等.固相萃取-超高效液相色谱-串联质谱法测定人指甲中的三氯生和三氯卡班[J].色谱,2013,31(11):1 040-1 045.
    [8]陈建华,彭刚华,乔支卫,等.固相萃取-超高效液相色谱法检测地表水中7种氯酚类化合物[J].中国环境监测,2015,31(3):144-149.
    [9]DAVID A,ABDUL-SADA A,LANGE A,et al.A New Approach for Plasma(xeno)Metabolomics Based on Solid-phase Extraction and Nanoflow Liquid Chromatography-nanoelectrospray Ionisation Mass Spectrometry[J].J Chromatogr A,2014,1365:72-85.
    [10]贾妍艳,谭建华,徐晨,等.固相萃取-气相色谱-质谱法同时测定水中9种药品及个人护理用品[J].色谱,2014,32(3):263-267.
    [11]韩超,黄芙珍,李舟,等.基于固相萃取-液相色谱-串联质谱法的纺织品中三氯生和三氯卡班的测定[J].纺织学报,2014,35(4):71-74.
    [12]吕庆,李海玉,李丕,等.气相色谱-串联质谱法测定木制儿童用品中的10种木材防腐剂[J].质谱学报,2013,34(6):321-329.
    [13]卢俊文,李蓉,杨芳,等.气相色谱-串联质谱法快速测定水果中咪鲜胺及其代谢物2,4,6-三氯苯酚的残留量[J].食品科学,2015,36(12):213-217.
    [14]CELANO R,PICCINELLI A L,CAMPONE L,et al.Ultra-preconcentration and Determination of Selected Pharmaceutical and Personal Care Products in Different Water Matrices by Solid-phase Extraction Combined with Dispersive Liquid-liquid Microextraction Prior to Ultra High Pressure Liquid Chromatography Tandem Mass Spectrometry Analysis[J].J Chromatogr A,2014,1355:26-35.
    [15]张品,张晶,陈洁君,等.在线固相萃取-超高效液相色谱-串联质谱法测定乳制品中双酚A等4种内分泌干扰物[J].分析化学,2014,42(12):1 811-1 817.
    [16]张品,张晶,石莹,等.固相萃取-超高效液相色谱-串联质谱法测定母乳中三氯生和三氯卡班[J].卫生研究,2015,44(2):294-298.
    [17]车文军,武中平,卢剑,等.固相萃取/高效液相色谱法同时测定化妆品中9种卤代酚残留[J].分析测试学报,2013,32(4):499-503.
    [18]PAN S D,ZHOU L X,ZHAO Y G,et al.Aminefunctional Magnetic Polymer Modified Graphene Oxide as Magnetic Solid-phase Extraction Materials Combined with Liquid Chromatography-tandem Mass Spectrometry for Chlorophenols Analysis in Environmental Water[J].J Chromatogr A,2014,1 362:34-42.
    [19]申书昌,徐雅雯,马柏凤.弱酸型聚合物微球固相萃取填料的制备及水中杀虫剂的测定[J].化学研究与应用,2015,27(9):1 289-1 294.
    [20]AZZOUZ A,BALLESTEROS E.Trace Analysis of Endocrine Disrupting Compounds in Environmental Water Samples by Use of Solid-phase Extraction and Gas Chromatography with Mass Spectrometry Detection[J].J Chromatogr A,2014,1 360:248-257.
    [21]ANUMOL T,SNYDER S A.Rapid Analysis of Trace Organic Compounds in Water by Automated Online Solid-phase Extraction Coupled to Liquid Chromatography-tandem Mass Spectrometry[J].Talanta,2015,132:77-86.
    [22]GUO F,LIU Q,SHI J B,et al.Direct Analysis of Eight Chlorophenols in Urine by Large Volume Injection Online Turbulent Flow Solid-phase Extraction Liquid Chromatography with Multiple Wavelength Ultraviolet Detection[J].Talanta,2014,119:396-400.
    [23]RAOOV M,MOHAMAD S,ABAS M R B,et al.New Macroporousβ-Cyclodextrin Functionalized Ionic Liquid Polymer as an Adsorbent for Solid Phase Extraction with Phenols[J].Talanta,2014,130:155-163.
    [24]GONZALO-LUMBRERAS R,SANZ-LANDALUZE J,CAMARA C.Analytical Performance of Two Miniaturised Extraction Methods for Triclosan and Methyltriclosan,in Fish Roe and Surimi Samples[J].Food Chem,2014,146:141-148.
    [25]LIU X L,WANG C,WU Q H,et al.Preconcentration of Chlorophenols in Water Samples Using Threedimensional Graphene-based Magnetic Nanocomposite as Absorbent[J].Chin Chem Lett,2014,25(8):1 185-1 189.
    [26]AZZOUZ A,RASCON A J,BALLESTEROS E.Simultaneous Determination of Parabens,Alkylphenols,Phenylphenols,Bisphenol A and Triclosan in Human Urine,Blood and Breast Milk by Continuous Solid-phase Extraction and Gas Chromatographymass Spectrometry[J].J Pharm Biomed Anal,2016,119:16-26.
    [27]BELARDI R P,PAWLISZYN J B.The Application of Chemically Modified Fused Silica Fibers in Extraction of Organics from Water Matrix Samples,and Their Rapid Transfer to Capillary Column[J].Water Pollut Res J Can,1989,24(1):179-191.
    [28]马继平,王涵文,关亚风.固相微萃取新技术[J].色谱,2002,20(1):16-20.
    [29]ALVAREZ-RIVERA G,VILA M,LORES M,et al.Development of a Multi-preservative Method Based on Solid-phase Microextraction-gas Chromatographytandem Mass Spectrometry for Cosmetic Analysis[J].J Chromatogr A,2014,1 339:13-25.
    [30]ABOLGHASEMI M M,YOUSEFI V.Three Dimensionally Honeycomb Layered Double Hydroxides Framework as a Novel Fiber Coating for Headspace Solid-phase Microextraction of Phenolic Compounds[J].J Chromatogr A,2014,1 345:9-16.
    [31]MEI M,HUANG X J,YUAN D X.Multiple Monolithic Fiber Solid-phase Microextraction:A Newextraction Approach for Aqueous Samples[J].J Chromatogr A,2014,1 345:29-36.
    [32]ZENG J B,ZHAO C Y,CHEN J J,et al.Ordered Mesoporous Carbon/Nafion as a Versatile and Selective Solid-phase Microextraction Coating[J].J Chromatogr A,2014,1 365:29-34.
    [33]YANG Y X,LIA Y,LIU H X,et al.Electrodeposition of Gold Nanoparticles onto an Etched Stainless Steel Wire Followed by a Self-assembled Monolayer of Octanedithiol as a Fiber Coating for Selective Solidphase Microextraction[J].J Chromatogr A,2014,1 372:25-33.
    [34]ABOLGHASEMIA M M,HASSANI S,RAFIEE E,et al.Nanoscale-supported Heteropoly Acid as a New Fiber Coating for Solid-phase Microextraction Coupled with Gas Chromatography-mass Spectrometry[J].J Chromatogr A,2015,1 381:48-53.
    [35]ALVAREZ-RIVERA G,LLOMPART M,GARCIAJARES C,et al.Identification of Unwanted Photoproducts of Cosmetic Preservatives in Personal Care Products under Ultraviolet-light Using Solid-phase Microextraction and Micro-matrix Solid-phase Dispersion[J].J Chromatogr A,2015,1 390:1-12.
    [36]GONG S X,WANG X,CHEN Y,et al.Carboxylated Solid Carbon Spheres as a Novel Solid-phase Microextraction Coating for Sensitive Determination of Phenols in Environmental Water Samples[J].J Chromatogr A,2015,1 401:17-23.
    [37]SARAJI M,GHANI M.Hollow Fiber Liquid-liquidliquid Microextraction Followed by Solid-phase Microextraction and in Situ Derivatization for the Determination of Chlorophenols by Gas Chromatography-electron Capture Detection[J].J Chromatogr A,2015,1 418:45-53.
    [38]HOLOPAINEN S,LUUKKONEN V,NOUSIAINEN M,et al.Determination of Chlorophenols in Water by Headspace Solid Phase Microextraction Ion Mobility Spectrometry(HS-SPME-IMS)[J].Talanta,2013,114:176-182.
    [39]FARHADI K,MARIN A A,AMANZADEH H,et al.A Novel Dispersive Micro Solid Phase Extraction Using Zein Nanoparticles as the Sorbent Combined with Headspace Solid Phase Micro-extraction to Determine Chlorophenols in Water and Honey Samples by GC-ECD[J].Talanta,2014,128:493-499.
    [40]ALIZADEH R.Chlorophenol’s Ultra-trace Analysis in Environmental Samples by Chitosan-zinc Oxide Nanorod Composite as a Novel Coating for Solid Phase Micro-extraction Combined with High Performance Liquid Chromatography[J].Talanta,2016,146:831-838.
    [41]ABOLGHASEMI M M,PARASTARI S,YOUSEFI V.Polypyrrole-montmorillonite Nano-composite as Sorbent for Solid-phase Microextraction of Phenolic Compounds in Water[J].J Sep Sci,2014,37(23):3 526-3 532.
    [42]ABOLGHASEMI M M,PARASTARI S,YOUSEFI V.Microextraction of Phenolic Compounds Using a Fiber Coated with a Polyaniline-montmorillonite Nanocomposite[J].Microchim Acta,2015,182(1):273-280.
    [43]ABOLGHASEMI M M,YOUSEFI V,AMIRSHAGHAGHI A.Preparation and Evaluation of a Layered Double Hydroxide Film on a Nanoporous Anodic Aluminum Oxide/Aluminum Wire as a Highly Thermalresistant Solid-phase Microextraction Fiber[J].New J Chem,2015,39(4):3 109-3 115.
    [44]ABOLGHASEMI M M,YOUSEFI V,PIRYAEI M.Synthesis of a Metal-organic Framework Confined in Periodic Mesoporous Silica with Enhanced Hydrostability as a Novel Fiber Coating for Solid-phase Microextraction[J].J Sep Sci,2015,38(7):1 187-1 193.
    [45]YANG Y X,GUO M,ZHANG Y D,et al.Self-assembly of Alkyldithiols on a Novel Dendritic Silver Nanostructure Electrodeposited on a Stainless Steel Wire as a Fiber Coating for Solid-phase Microextraction[J].RSC Adv,2015,5(88):71 859-71 867.
    [46]HUANG X J,ZHANG Y,MEI M,et al.Preparation of Monolithic Fibers for the Solid-phase Microextraction of Chlorophenols in Water Samples[J].J Sep Sci,2014,37(9-10),1 185-1 193.
    [47]HE H,ZHUANG Y,PENG Y,et al.Solid-phase Microextraction Based on Polyaniline Doped with Perfluorooctanesulfonic Acid Coupled to HPLC for the Quantitative Determination of Chlorophenols in Water Samples[J].J Sep Sci,2014,37(4):427-433.
    [48]BAGHERI H,NAJARZADEKAN H,ROOSTAIE A.Electrospun Polyamide-polyethylene Glycol Nanofibers for Headspace Solid-phase Microextration[J].J Sep Sci,2014,37(14):1 880-1 886.
    [49]SUN M,BU Y N,FENG J J,et al.Graphene Oxide Reinforced Polymeric Ionic Liquid Monolith Solidphase Microextraction Sorbent for High-performance Liquid Chromatography Analysis of Phenolic Compounds in Aqueous Environmental Samples[J].J Sep Sci,2016,39(2):375-382.
    [50]JEANNOT M A,CANTWELL F F.Solvent Microextraction into a Single Drop[J].Anal Chem,1996,68(13):2 236-2 240.
    [51]JEANNOT M A,CANTWELL F F.Mass Transfer Characteristics of Solvent Extraction into a Single Drop at the Tip of a Syringe Needle[J].Anal Chem,1997,69(2):235-239.
    [52]GE D,LEE H K.Ultra-hydrophobic Ionic Liquid 1-Hexyl-3-methylimidazolium Tris(pentafluoroethyl)Trifluorophosphate Supported Hollow-fiber Membrane Liquid-liquid-liquid Microextraction of Chlorophenols[J].Talanta,2015,132:132-136.
    [53]FAN C,LI N,CAO X L.Determination of Chlorophenols in Honey Samples Using in-situ Ionic Liquiddispersive Liquid-liquid Microextraction as a Pretreatment Method Followed by High-performance Liquid Chromatography[J].Food Chem,2015,174:446-451.
    [54]WANG K D,CHEN P S,HUANG S D.Simultaneous Derivatization and Extraction of Chlorophenols in Water Samples with up-and-down Shaker-assisted Dispersive Liquid-liquid Microextraction Coupled with Gas Chromatography/mass Spectrometric Detection[J].Anal Bioanal Chem,2014,406(8):2 123-2 131.
    [55]GONZALEZ A,AVIVAR J,CERDA V.Determination of Priority Phenolic Pollutants Exploiting an Insyringe Dispersive Liquid-liquid Microextraction-multisyringe Chromatography System[J].Anal Bioanal Chem,2015,407(7):2 013-2 022.
    [56]ZHANG M,CHENG J,WU M,et al.Gas Chromatographic Determination of Three Chlorophenols in Toilet Paper by Ultrasonic Assisted Extraction and Synchronous Derivative Dispersive Liquid-liquid Microextraction[J].Anal Methods,2014,6(1):207-214.
    [57]FAN Y Y,HU S B,LIU S H.Salting-Out Assisted Liquid-liquid Extraction Coupled to Dispersive Liquidliquid Microextraction for the Determination of Chlorophenols in Wine by High-performance Liquid Chromatography[J].J Sep Sci,2014,37(24):3 662-3 668.
    [58]SUN M,CUI P L,JI S J,et al.Octadecyl-modified Graphene as an Adsorbent for Hollow Fiber Liquid Phase Microextraction of Chlorophenols from Honey[J].Bull Korean Chem Soc,2014,35(4):1 011-1 015.
    [59]周新,杨迎春,叶芝祥.反乳化分散液液微萃取-HPLC测定水中二氯酚[J].环境科学与技术,2015,38(5):90-94,101.
    [60]孙建芝,贺晖,刘书慧.分散液液微萃取-反相液液微萃取-扫集-胶束电动色谱法测定红酒中的3种氯酚类物质[J].色谱,2014,32(3):256-262.
    [61]LEE H R,CHO S M,KIM J,et al.Novel and Simple Headspace in-Tube Microextraction Coupled with Capillary Electrophoresis[J].J Chromatogr A,2014,1 346:117-122.
    [62]SLAMPOVA A,KUBAN P,BOCEK P.Effects of Selected Operational Parameters on Efficacy and Selectivity of Electromembrane Extraction.Chlorophenols as Model Analytes[J].Electrophoresis,2014,35(17):2 429-2 437.
    [63]WEI X,ZHOU Z P,DAI J D,et al.Composites of Surface Imprinting Polymer Capped Mn-doped ZnS Quantum Dots for Room-temperature Phosphorescence Probing of 2,4,5-Trichlorophenol[J].J Lumin,2014,155:298-304.
    [64]QI S D,ZHANG H G,ZHU Q,et al.Off-line Hyphenation of Molecularly Imprinted Magnetic Nanoparticle-based Extraction with Large Volume Sample Stacking Capillary Electrophoresis for High-sensitivity Detection of Trace Chlorophenols[J].Anal Methods,2014,6(4):1 219-1 226.
    [65]CACHO J I,CAMPILLO N,VINAS P,et al.Stir Bar Sorptive Extraction Polar Coatings for the Determination of Chlorophenols and Chloroanisoles in Wines Using Gas Chromatography and Mass Spectrometry[J].Talanta,2014,118:30-36.
    [66]王成云,李丽霞,张伟亚,等.微波辅助萃取/气相色谱法测定抗菌纺织品中的三氯生[J].应用化学,2012,29(1):118-122.
    [67]PAREDES R M G,PINTO C G,PAVON J L P,et al.In Situ Derivatization Combined to Automated Microextraction by Packed Sorbents for the Determination of Chlorophenols in Soil Samples by Gas Chromatography Mass Spectrometry[J].J Chromatogr A,2014,1359:52-59.
    [68]王新鑫,杨军,谢晟瑜,等.基于分子印迹磁性复合材料的基质分散-固相萃取/液相色谱法测定海水中的氯酚类污染物[J].分析测试学报,2015,34(11):1 213-1 219.
    [69]江静,邵晓玲,常真,等.中空纤维支载离子液体液液微萃取法检测环境水体中的三氯生[J].分析化学,2012,40(8):1 257-1 261.
    [70]杨秋红,程小艳,杨坪,等.固相萃取-高效液相色谱串联质谱法同时检测地表水中的2,4-二氯酚、2,4,6-三氯酚和五氯酚[J].分析化学,2011,39(8):1 208-1 212.
    [71]王天娇,林勤保,宋欢,等.超高效液相色谱-串联质谱法测定食品包装纸中的酚类化合物[J].分析测试学报,2010,29(12):1 153-1 157.
    [72]金米聪,颜勇卿,陈晓红,等.离子色谱-质谱联用法同时测定饮用水中3种痕量一氯酚[J].分析化学,2006,34(9):1 223-1 226.
    [73]FERREIRA A M C,MODER M,LAESPADAM E F.GC-MS Determination of Parabens,Triclosan and Methyl Triclosan in Water by in Situ Derivatisation and Stir-bar sorptive Extraction[J].Anal Bioanol Chem,2011,399(2):945-953.
    [74]于雄胜,柳勇,楼骏,等.涡旋辅助-液液萃取-气相色谱法测定土壤中水和甲醇可提态五氯酚[J].分析化学,2015,43(9):1 389-1 394.
    [75]姜乃琪,佟丽丽,姜东娇,等.不同土壤对水体中4-氯酚的吸附行为研究[J].沈阳师范大学学报(自然科学版),2014,32(4):506-509.
    [76]肖宇芳,刘广民,董永亮,等.土壤中五氯酚的快速测定[J].岩矿测试,2008,27(2):117-119.
    [77]杨冰仪,莫金垣,邹小勇,等.双通道毛细管电泳-电化学法同时检测硝酸根、亚硝酸根和氯酚类化合物[J].应用化学,2005,22(5):484-488.
    [78]WEI M C,TIAN D,LIU S,et al.β-Cyclodextrin Functionalized Graphene Material:A Novel Electrochemical Sensor for Simultaneous Determination of 2-Chlorophenol and 3-Chlorophenol[J].Sens Actuators B,2014,195:452-458.
    [79]ZHANG Y Y,CHENG Q,ZHENG M,et al.Iron Oxyhydroxide Nanorods with High Electrochemical Reactivity as a Sensitive and Rapid Determination Platform for 4-Chlorophenol[J].J Hazard Mater,2016,307:36-42.
    [80]ZHU Y Y,WU M M,LIU S T.Self-assembly of Ag-Phosphotungstic Acid Composite Nanoparticles on a Modified ITO Electrode for the Electrochemical Detection of 4-Chlorophenol[J].J Appl Electrochem,2013,43(10):1 035-1 041.
    [81]NOGUERA P,MAQUIEIRA A,PUCHADES R,et al.Development of an Enzyme-linked Immunosorbent Assay for Pentachlorophenol[J].Anal Chim Acta,2002,460(2):279-288.
    [82]余宇燕,庄惠生.环境激素类物质2,4-二氯苯酚荧光免疫分析方法的建立[J].分析测试学报,2008,27(6):607-610.
    [83]NICHKOVA M,FENG J,SANCHEZ-BAEZE F,et al.Competitive Quenching Fluorescence Immunoassay for Chlorophenols Based on Laser-induced Fluorescence Detection in Microdroplets[J].Anal Chem,2003,75(1):83-90.
    [84]姚英华,李娟秀,陈贝贝,等.采用荧光探针测定五氯酚[J].化学传感器,2011,31(3):49-53.
    [85]HE H,LIU S H,MENG Z F,et al.Dispersive Liquid-liquid Microextraction for the Determination of Phenols by Acetonitrile Stacking Coupled with Sweepingmicellar Electrokinetic Chromatography with Largevolume Injection[J].J Chromatogr A,2014(36):291-298.

© 2004-2018 中国地质图书馆版权所有 京ICP备05064691号 京公网安备11010802017129号

地址:北京市海淀区学院路29号 邮编:100083

电话:办公室:(+86 10)66554848;文献借阅、咨询服务、科技查新:66554700