惰气熔融-红外吸收/热导法在无机固态材料气体分析中的应用
|
摘要
综述了近十年来惰气熔融-红外吸收/热导法在金属合金、稀土材料、冶金添加剂、耐火陶瓷等无机固态材料气体元素分析中的应用现状,侧重汇总了称样量、助熔剂、分析功率、标准样品等主要分析条件,介绍了氢、氧、氮元素分量测定的最新进展。讨论了该法存在的问题,并提出相关建议,展望了无机固态材料中气体分析的应用前景和发展方向。
The application status for gas analysis of inorganic solid materials,including metal alloys,rare earth materials,metallurgical additives and refractory ceramic,was reviewed by inert gas fusioninfrared absorption or thermal conductivity method.The main analytical conditions,such as sample mass,flux,analytical power and certified reference materials,were specially summarized,and the latest progress on the determination of partial hydrogen,oxygen and nitrogen was introduced.At last,the demerits of these two methods were discussed,and the related suggestions were proposed.Simultaneously,the application prospect and development of gas analysis in inorganic solid materials were forecasted.
The application status for gas analysis of inorganic solid materials,including metal alloys,rare earth materials,metallurgical additives and refractory ceramic,was reviewed by inert gas fusioninfrared absorption or thermal conductivity method.The main analytical conditions,such as sample mass,flux,analytical power and certified reference materials,were specially summarized,and the latest progress on the determination of partial hydrogen,oxygen and nitrogen was introduced.At last,the demerits of these two methods were discussed,and the related suggestions were proposed.Simultaneously,the application prospect and development of gas analysis in inorganic solid materials were forecasted.
引文
[1]胡少成,沈学静,王蓬.固态金属及合金材料中氧、氮、氢联测技术进展[J].冶金分析(Metallurgical Analysis),2009,29(11):34-40.
[2]高巍,赵宇,王丽晖,等.钢中氢的分析方法优化[J].冶金分析(Metallurgical Analysis),2007,27(9):57-59.
[3]朱跃进,孙明月,李素娟,等.定氢钢样制备方法研究[J].冶金分析(Metallurgical Analysis),2013,33(7):16-20.
[4]张长均,王蓬,杨植岗,等.无舒茨试剂测定钛中氢[C]//中国金属学会第十二届分析测试学术年会论文集,北京:出版地不详,2004:366-367.
[5]何雄杰.钛及钛合金中氧和氢的联合测定[J].钛工业进展(Titanium Industry Progress),2006,23(1):32-34.
[6]张小英,张藏淑,廖丽红,等.测定非晶合金带中氢含量[J].冶金分析(Metallurgical Analysis),2001,21(6):51-53.
[7]朱跃进,李素娟.惰气熔融法测定镁中氧、氢、氮[J].冶金分析(Metallurgical Analysis),2011,31(12):58-61.
[8]李素娟,朱跃进.脉冲热导法测定铝及铝合金中氢[J].冶金分析(Metallurgical Analysis),2002,22(5):58-59.
[9]钟华.脉冲加热-红外吸收光谱法测定钒铝合金中氢[J].中国无机分析化学(Chinese Journal of Inorganic Analytical Chemistry),2013,3(2):56-59.
[10]程晓舫,缪琳.惰气熔融-热导法测定电解锰中氢[J].安徽冶金科技职业学院学报(Journal of Anhui Vocational College of Metallurgy and Technology),2005,15(1):31-32.
[11]蒋亚芳,张杰,苏兴智.脉冲加热-红外法测定钽、铌中氢量[J].硬质合金(Cemented Carbide),2010,27(6):376-379.
[12]邹乐西,李英秋,刘钧,等.影响铀铌合金中微量氢测定的因素研究[J].核化学与放射化学(Journal of Nuclear and Radiochemistry),2002,24(1):26-29.
[13]ASTM E1019-2011 Standard test methods for determination of carbon,sulfur,nitrogen,and oxygen in steel,iron,nickel,and cobalt alloys by various combustion and fusion techniques[S].
[14]ASTM E1409-2013 Standard test method for determination of oxygen and nitrogen in titanium and titanium alloys by inert gas fusion[S].
[15]郭少毅.用基准试剂作标准测定钢中微量氧[J].冶金分析(Metallurgical Analysis),2000,20(4):66,55.
[16]王伟,曹忠孝,王俊.惰气熔融-热导法测定钛铁中氮[J].冶金分析(Metallurgical Analysis),2010,30(9):62-64.
[17]张瑞霖,郭燕青,梁敏鉴.脉冲加热熔融热导法测定钛铁合金中氮含量[J].冶金分析(Metallurgical Analysis),2010,30(8):25-29.
[18]马红权,王学华,王蓬,等.低温投样提高锡铅合金中氧含量测定的精密度[C]//中国金属学会第十三届冶金及材料分析测试学术报告会论文集,北京:出版地不详,2006:229-230.
[19]Tsuge A,Achiwa H,Morikawa H,et al.Determination of oxygen content in magnesium and its alloys by inert gas fusion-infrared absorptiometry[J].Anal.Sci.,2011,27(7):721.
[20]钱庆长,骆友健.脉冲加热红外吸收法测定雾化铜粉中氧[J].冶金分析(Metallurgical Analysis),2004,24(6):44-46.
[21]方卫,刘伟,等.高温钛合金粉中氧氮的同时测定[J].分析试验室(Chinese Journal of Analysis Laboratory),2001,20(6):94-95.
[22]郇枚.钢中氧氮的测定[C]//中国金属学会第十二届分析测试学术年会论文集,北京:出版地不详,2004:423-424.
[23]周岭,郑华,周海收.镍锰钴合金中氧的测定方法研究[J].稀有金属(Chinese Journal of Rare Metals),2002,26(4):287-289.
[24]石新层,周恺,杨军红.惰气熔融-红外热导法同时测定铌钛合金中氧和氮[J].冶金分析(Metallurgical Analysis),2010,30(12):30-32.
[25]周海收,宋晓力,王洪斌,等.铜的铬、钼、钨合金中杂质氧、氮的测定方法研究[J].分析试验室(Chinese Journal of Analysis Laboratory),2007,26(1):93-96.
[26]王启芳,周海收,赵振庚,等.锡铅银等低熔点合金中氧的测定方法研究[J].分析试验室(Chinese Journal of Analysis Laboratory),2002,21(5):66-68.
[27]耿小颖,张克顺,杨春晟,等.脉冲加热-红外吸收、热导法测定粉末高温合金中氧、氮[J].分析试验室(Chinese Journal of Analysis Laboratory),2009,28(z1):303-306.
[28]杨国荣.脉冲加热-惰性气体熔融-红外吸收法测定Bi粉中总氧含量[C]//中国金属学会第十三届冶金及材料分析测试学术报告会论文集,北京:出版地不详,2006:253-256.
[29]刘伟,刘文,韩守礼,等.脉冲红外和热导检测法测定钌粉和钌靶中氧、氮含量[J].贵金属(Precious Metals),2013,34(4):53-56.
[30]GB/T 12690.4-2003稀土金属及其氧化物中非稀土杂质化学分析方法氧、氮量的测定脉冲-红外吸收法脉冲-热导法[S].
[31]高光洁子,冯圣雅,王莘泉,等.惰气熔融-脉冲加热法同时测定NdFeB合金中氧和氮[J].冶金分析(Metallurgical Analysis),2011,31(1):30-34.
[32]周海收,王启芳.氟化钕中杂质氧、氮的测定方法研究[J].稀有金属(Chinese Journal of Rare Metals),2004,28(6):1103-1105.
[33]周海收,王启芳.稀土金属钕和镝中氧氮的测定方法研究[J].分析试验室(Chinese Journal of Analysis Laboratory),2005,24(3):79-81.
[34]杨倩倩,张长均,赵雷,等.惰气熔融-红外光谱法测定镨钕镝中的氧[J].中国无机分析化学(Chinese Journal of Inorganic Analytical Chemistry),2013,3(2):60-62.
[35]周海收,王启芳.混合稀土储氢合金中氧和氮的测定[J].分析试验室(Chinese Journal of Analysis Laboratory),2006,25(10):83-85.
[36]吴伦强,邹乐西,向方寿,等.同时测定铀铌合金中微量氧和氮[J].理化检验-化学分册(Physical Testing and Chemical Analysis Part B:Chemical Analysis),2001,37(3):102-103.
[37]孙金库,秦毅,王树安.红外吸收法和热导法测定铀钼合金中氧和氮[J].冶金分析(Metallurgical Analysis),2010,30(5):6-8.
[38]杨帆.脉冲红外法测定碳素铬铁焙烧料中氧[C]//中国金属学会第十二届分析测试学术年会论文集,北京:出版地不详,2004:371-373.
[39]钟华.惰气熔融-热导法测定氮化铬铁中氮[J].冶金分析(Metallurgical Analysis),2010,30(3):64-67.
[40]何克伦,董敏,华雁芬.脉冲加热-热导法测定氮化锰粉末中的氮含量[J].化学分析计量(Chemical Analysis and Meterage),2010,19(4):48-49.
[41]杨帆.惰气熔融-热导法测定氮化硅铁中氮[J].冶金分析(Metallurgical Analysis),2008,28(5):78-80.
[42]程晓舫,程坚平,杨劲松.惰气熔融-热导法测定钒氮合金中氮[J].冶金分析(Metallurgical Analysis),2004,24(2):68-69.
[43]王蓬,杨帆,李宏伟,等.钒氮合金中高氮检测的新方法[J].钢铁钒钛(Iron Steel Vanadium Titanium),2005,26(3):64-68.
[44]李岩,王强.铝钒合金中氧含量测定方法的研究[J].分析试验室(Chinese Journal of Analysis Laboratory),2010,29(z1):331-333.
[45]方南辉,张水菊,段清国,等.低氮增碳剂中氮的检测方法研究[J].江西冶金(Jiangxi Metallurgy),2010,30(6):39-41,46.
[46]朱跃进,李素娟.惰气熔融-热导法测定烧结氮化硅中氮[J].冶金分析(Metallurgical Analysis),2001,21(2):1-3.
[47]顾春峰,邬君飞.耐火材料中氮的测定[C]//中国金属学会第十二届分析测试学术年会论文集,北京:出版地不详,2004:401-402.
[48]王伟,曹忠孝,王俊.惰气熔融-热导法测定金属硅中氮[J].冶金分析(Metallurgical Analysis),2008,28(2):66-68.
[49]王蓬,杨植岗,吴振宁,等.氮化硅中超高氮的检测[C]//第七届中国钢铁年会论文集,北京:出版地不详,2009:5166-5170.
[50]曹海洁.熔融热导法测定含氮耐火材料中的总氮量[J].耐火材料(Refractories),2006,40(2):145-146.
[51]何克伦,董敏,华雁芬,等.脉冲加热-红外法测定超细二硅化钼粉末中氧[J].分析科学学报(Journal of Analytical Science),2009,25(6):735-737.
[52]何克伦,华雁芬,董敏,等.红外吸收法测定碳化铪粉末中的氧含量[J].化学分析计量(Chemical Analysis and Meterage),2010,19(1):58-59.
[53]钟华.惰气熔融-热导法测定碳化钽粉中氮[J].冶金分析(Metallurgical Analysis),2013,33(1):43-45.
[54]华雁芬,董敏,何克伦,等.连续碳化硅纤维中氧和氮的测定[C]//中国金属学会第十六届国际冶金及材料分析测试学术报告会论文集,北京:出版地不详,2012:849-851.
[55]王兴其,杨毅.2091铝-锂合金固态氢含量的测定[J].光谱学与光谱分析(Spectroscopy and Spectral Analysis),2000,20(1):125-127.
[56]赵洋,王强,张克顺.脉冲加热-热导法测定高锌铝合金中氢含量[J].化学分析计量(Chemical Analysis and Meterage),2011,20(4):45-47.
[57]白周建.金属材料表层氢的相对测定[J].火箭推进(Journal of Rocket Propulsion),2008,34(2):41-44.
[58]王瑞珍,杨继东.惰气熔融红外法测定钢铁试样表面氧和体内氧[J].金属材料与冶金工程(Metal Materials and Metallurgy Engineering),2010,38(1):44-48,51.
[59]沈汝美,陈名浩.钢中氧化物夹杂差热抽取峰形分离研究[J].分析化学(Chinese Journal of Analytical Chemistry),2000,10(3):337-341.
[60]王健春,安静,丁美英,等.差热法快速测定钢中氧化夹杂的初探[J].冶金分析(Metallurgical Analysis),2002,22(1):33-35.
[61]李素娟,朱跃进.惰气熔融程序升温法测定氧氮分量图谱分析[C]//中国金属学会第十二届分析测试学术年会论文集,北京:出版地不详,2004:418-420.
[62]程晓舫,程坚平,姚鑫.氧氮分析仪测定钢中氮化物分量的初探[C]//中国金属学会第十三届冶金及材料分析测试学术报告会论文集,北京:出版地不详,2006:260-264.
[63]王蓬,杨植岗,王海舟.钕铁硼中不同状态氧释放行为的研究[J].冶金分析(Metallurgical Analysis),2007,27(6):1-7.
[64]朱跃进.脉冲红外法测定纳米材料中总氧和氧分量[J].冶金分析(Metallurgical Analysis),2003,23(2):11-13,19.
[65]朱跃进.不同程序脉冲升温条件下一些纳米粉体中氧的释放行为[J].冶金分析(Metallurgical Analysis),2006,26(1):13-16.
[66]王峰,杨红忠.脉冲红外法测定钼粉中氧含量及其分量研究[J].稀有金属(Chinese Journal of Rare Metals),2003,27(1):205-206.
[67]王瑞珍.硅铁等粉料中氧分量测定的初步研究[J].冶金分析(Metallurgical Analysis),2005,25(3):16-21.
[68]杨会珍.阶梯式程序升温测定硬质合金混合料中总氧量和氧分量[J].中国无机分析化学(Chinese Journal of Inorganic Analytical Chemistry),2012,2(2):41-44.
[69]沈学静,王蓬,胡少成,等.脉冲熔融-飞行时间质谱法测定金属材料中氧、氮、氢和氩[J].分析化学(Chinese Journal of Analytical Chemistry).2011,39(10):1555-1560.
[70]Shen X,Wang P,Hu S,et al.Simultaneous determination of oxygen,nitrogen and hydrogen in metals by pulse heating and time of flight mass spectrometric method[J].Talanta.2011,84(4):1057-1062.
[71]马爱方.火花源发射光谱仪测定钢中的氧[J].河北冶金(Hebei Metallurgy),2003(6):53-55.
[72]刘辉,张春晓,胡军,等.火花源原子发射光谱法测定NiFeCr合金中氮[J].冶金分析(Metallurgical Analysis),2012,32(6):10-13.
[73]Laur F,Carolina D A.阿塞洛米塔尔图巴朗钢铁集团火花发射光谱法优化氮的分析[J].冶金分析(Metallurgical Analysis),2012,32(7):25-31.
[2]高巍,赵宇,王丽晖,等.钢中氢的分析方法优化[J].冶金分析(Metallurgical Analysis),2007,27(9):57-59.
[3]朱跃进,孙明月,李素娟,等.定氢钢样制备方法研究[J].冶金分析(Metallurgical Analysis),2013,33(7):16-20.
[4]张长均,王蓬,杨植岗,等.无舒茨试剂测定钛中氢[C]//中国金属学会第十二届分析测试学术年会论文集,北京:出版地不详,2004:366-367.
[5]何雄杰.钛及钛合金中氧和氢的联合测定[J].钛工业进展(Titanium Industry Progress),2006,23(1):32-34.
[6]张小英,张藏淑,廖丽红,等.测定非晶合金带中氢含量[J].冶金分析(Metallurgical Analysis),2001,21(6):51-53.
[7]朱跃进,李素娟.惰气熔融法测定镁中氧、氢、氮[J].冶金分析(Metallurgical Analysis),2011,31(12):58-61.
[8]李素娟,朱跃进.脉冲热导法测定铝及铝合金中氢[J].冶金分析(Metallurgical Analysis),2002,22(5):58-59.
[9]钟华.脉冲加热-红外吸收光谱法测定钒铝合金中氢[J].中国无机分析化学(Chinese Journal of Inorganic Analytical Chemistry),2013,3(2):56-59.
[10]程晓舫,缪琳.惰气熔融-热导法测定电解锰中氢[J].安徽冶金科技职业学院学报(Journal of Anhui Vocational College of Metallurgy and Technology),2005,15(1):31-32.
[11]蒋亚芳,张杰,苏兴智.脉冲加热-红外法测定钽、铌中氢量[J].硬质合金(Cemented Carbide),2010,27(6):376-379.
[12]邹乐西,李英秋,刘钧,等.影响铀铌合金中微量氢测定的因素研究[J].核化学与放射化学(Journal of Nuclear and Radiochemistry),2002,24(1):26-29.
[13]ASTM E1019-2011 Standard test methods for determination of carbon,sulfur,nitrogen,and oxygen in steel,iron,nickel,and cobalt alloys by various combustion and fusion techniques[S].
[14]ASTM E1409-2013 Standard test method for determination of oxygen and nitrogen in titanium and titanium alloys by inert gas fusion[S].
[15]郭少毅.用基准试剂作标准测定钢中微量氧[J].冶金分析(Metallurgical Analysis),2000,20(4):66,55.
[16]王伟,曹忠孝,王俊.惰气熔融-热导法测定钛铁中氮[J].冶金分析(Metallurgical Analysis),2010,30(9):62-64.
[17]张瑞霖,郭燕青,梁敏鉴.脉冲加热熔融热导法测定钛铁合金中氮含量[J].冶金分析(Metallurgical Analysis),2010,30(8):25-29.
[18]马红权,王学华,王蓬,等.低温投样提高锡铅合金中氧含量测定的精密度[C]//中国金属学会第十三届冶金及材料分析测试学术报告会论文集,北京:出版地不详,2006:229-230.
[19]Tsuge A,Achiwa H,Morikawa H,et al.Determination of oxygen content in magnesium and its alloys by inert gas fusion-infrared absorptiometry[J].Anal.Sci.,2011,27(7):721.
[20]钱庆长,骆友健.脉冲加热红外吸收法测定雾化铜粉中氧[J].冶金分析(Metallurgical Analysis),2004,24(6):44-46.
[21]方卫,刘伟,等.高温钛合金粉中氧氮的同时测定[J].分析试验室(Chinese Journal of Analysis Laboratory),2001,20(6):94-95.
[22]郇枚.钢中氧氮的测定[C]//中国金属学会第十二届分析测试学术年会论文集,北京:出版地不详,2004:423-424.
[23]周岭,郑华,周海收.镍锰钴合金中氧的测定方法研究[J].稀有金属(Chinese Journal of Rare Metals),2002,26(4):287-289.
[24]石新层,周恺,杨军红.惰气熔融-红外热导法同时测定铌钛合金中氧和氮[J].冶金分析(Metallurgical Analysis),2010,30(12):30-32.
[25]周海收,宋晓力,王洪斌,等.铜的铬、钼、钨合金中杂质氧、氮的测定方法研究[J].分析试验室(Chinese Journal of Analysis Laboratory),2007,26(1):93-96.
[26]王启芳,周海收,赵振庚,等.锡铅银等低熔点合金中氧的测定方法研究[J].分析试验室(Chinese Journal of Analysis Laboratory),2002,21(5):66-68.
[27]耿小颖,张克顺,杨春晟,等.脉冲加热-红外吸收、热导法测定粉末高温合金中氧、氮[J].分析试验室(Chinese Journal of Analysis Laboratory),2009,28(z1):303-306.
[28]杨国荣.脉冲加热-惰性气体熔融-红外吸收法测定Bi粉中总氧含量[C]//中国金属学会第十三届冶金及材料分析测试学术报告会论文集,北京:出版地不详,2006:253-256.
[29]刘伟,刘文,韩守礼,等.脉冲红外和热导检测法测定钌粉和钌靶中氧、氮含量[J].贵金属(Precious Metals),2013,34(4):53-56.
[30]GB/T 12690.4-2003稀土金属及其氧化物中非稀土杂质化学分析方法氧、氮量的测定脉冲-红外吸收法脉冲-热导法[S].
[31]高光洁子,冯圣雅,王莘泉,等.惰气熔融-脉冲加热法同时测定NdFeB合金中氧和氮[J].冶金分析(Metallurgical Analysis),2011,31(1):30-34.
[32]周海收,王启芳.氟化钕中杂质氧、氮的测定方法研究[J].稀有金属(Chinese Journal of Rare Metals),2004,28(6):1103-1105.
[33]周海收,王启芳.稀土金属钕和镝中氧氮的测定方法研究[J].分析试验室(Chinese Journal of Analysis Laboratory),2005,24(3):79-81.
[34]杨倩倩,张长均,赵雷,等.惰气熔融-红外光谱法测定镨钕镝中的氧[J].中国无机分析化学(Chinese Journal of Inorganic Analytical Chemistry),2013,3(2):60-62.
[35]周海收,王启芳.混合稀土储氢合金中氧和氮的测定[J].分析试验室(Chinese Journal of Analysis Laboratory),2006,25(10):83-85.
[36]吴伦强,邹乐西,向方寿,等.同时测定铀铌合金中微量氧和氮[J].理化检验-化学分册(Physical Testing and Chemical Analysis Part B:Chemical Analysis),2001,37(3):102-103.
[37]孙金库,秦毅,王树安.红外吸收法和热导法测定铀钼合金中氧和氮[J].冶金分析(Metallurgical Analysis),2010,30(5):6-8.
[38]杨帆.脉冲红外法测定碳素铬铁焙烧料中氧[C]//中国金属学会第十二届分析测试学术年会论文集,北京:出版地不详,2004:371-373.
[39]钟华.惰气熔融-热导法测定氮化铬铁中氮[J].冶金分析(Metallurgical Analysis),2010,30(3):64-67.
[40]何克伦,董敏,华雁芬.脉冲加热-热导法测定氮化锰粉末中的氮含量[J].化学分析计量(Chemical Analysis and Meterage),2010,19(4):48-49.
[41]杨帆.惰气熔融-热导法测定氮化硅铁中氮[J].冶金分析(Metallurgical Analysis),2008,28(5):78-80.
[42]程晓舫,程坚平,杨劲松.惰气熔融-热导法测定钒氮合金中氮[J].冶金分析(Metallurgical Analysis),2004,24(2):68-69.
[43]王蓬,杨帆,李宏伟,等.钒氮合金中高氮检测的新方法[J].钢铁钒钛(Iron Steel Vanadium Titanium),2005,26(3):64-68.
[44]李岩,王强.铝钒合金中氧含量测定方法的研究[J].分析试验室(Chinese Journal of Analysis Laboratory),2010,29(z1):331-333.
[45]方南辉,张水菊,段清国,等.低氮增碳剂中氮的检测方法研究[J].江西冶金(Jiangxi Metallurgy),2010,30(6):39-41,46.
[46]朱跃进,李素娟.惰气熔融-热导法测定烧结氮化硅中氮[J].冶金分析(Metallurgical Analysis),2001,21(2):1-3.
[47]顾春峰,邬君飞.耐火材料中氮的测定[C]//中国金属学会第十二届分析测试学术年会论文集,北京:出版地不详,2004:401-402.
[48]王伟,曹忠孝,王俊.惰气熔融-热导法测定金属硅中氮[J].冶金分析(Metallurgical Analysis),2008,28(2):66-68.
[49]王蓬,杨植岗,吴振宁,等.氮化硅中超高氮的检测[C]//第七届中国钢铁年会论文集,北京:出版地不详,2009:5166-5170.
[50]曹海洁.熔融热导法测定含氮耐火材料中的总氮量[J].耐火材料(Refractories),2006,40(2):145-146.
[51]何克伦,董敏,华雁芬,等.脉冲加热-红外法测定超细二硅化钼粉末中氧[J].分析科学学报(Journal of Analytical Science),2009,25(6):735-737.
[52]何克伦,华雁芬,董敏,等.红外吸收法测定碳化铪粉末中的氧含量[J].化学分析计量(Chemical Analysis and Meterage),2010,19(1):58-59.
[53]钟华.惰气熔融-热导法测定碳化钽粉中氮[J].冶金分析(Metallurgical Analysis),2013,33(1):43-45.
[54]华雁芬,董敏,何克伦,等.连续碳化硅纤维中氧和氮的测定[C]//中国金属学会第十六届国际冶金及材料分析测试学术报告会论文集,北京:出版地不详,2012:849-851.
[55]王兴其,杨毅.2091铝-锂合金固态氢含量的测定[J].光谱学与光谱分析(Spectroscopy and Spectral Analysis),2000,20(1):125-127.
[56]赵洋,王强,张克顺.脉冲加热-热导法测定高锌铝合金中氢含量[J].化学分析计量(Chemical Analysis and Meterage),2011,20(4):45-47.
[57]白周建.金属材料表层氢的相对测定[J].火箭推进(Journal of Rocket Propulsion),2008,34(2):41-44.
[58]王瑞珍,杨继东.惰气熔融红外法测定钢铁试样表面氧和体内氧[J].金属材料与冶金工程(Metal Materials and Metallurgy Engineering),2010,38(1):44-48,51.
[59]沈汝美,陈名浩.钢中氧化物夹杂差热抽取峰形分离研究[J].分析化学(Chinese Journal of Analytical Chemistry),2000,10(3):337-341.
[60]王健春,安静,丁美英,等.差热法快速测定钢中氧化夹杂的初探[J].冶金分析(Metallurgical Analysis),2002,22(1):33-35.
[61]李素娟,朱跃进.惰气熔融程序升温法测定氧氮分量图谱分析[C]//中国金属学会第十二届分析测试学术年会论文集,北京:出版地不详,2004:418-420.
[62]程晓舫,程坚平,姚鑫.氧氮分析仪测定钢中氮化物分量的初探[C]//中国金属学会第十三届冶金及材料分析测试学术报告会论文集,北京:出版地不详,2006:260-264.
[63]王蓬,杨植岗,王海舟.钕铁硼中不同状态氧释放行为的研究[J].冶金分析(Metallurgical Analysis),2007,27(6):1-7.
[64]朱跃进.脉冲红外法测定纳米材料中总氧和氧分量[J].冶金分析(Metallurgical Analysis),2003,23(2):11-13,19.
[65]朱跃进.不同程序脉冲升温条件下一些纳米粉体中氧的释放行为[J].冶金分析(Metallurgical Analysis),2006,26(1):13-16.
[66]王峰,杨红忠.脉冲红外法测定钼粉中氧含量及其分量研究[J].稀有金属(Chinese Journal of Rare Metals),2003,27(1):205-206.
[67]王瑞珍.硅铁等粉料中氧分量测定的初步研究[J].冶金分析(Metallurgical Analysis),2005,25(3):16-21.
[68]杨会珍.阶梯式程序升温测定硬质合金混合料中总氧量和氧分量[J].中国无机分析化学(Chinese Journal of Inorganic Analytical Chemistry),2012,2(2):41-44.
[69]沈学静,王蓬,胡少成,等.脉冲熔融-飞行时间质谱法测定金属材料中氧、氮、氢和氩[J].分析化学(Chinese Journal of Analytical Chemistry).2011,39(10):1555-1560.
[70]Shen X,Wang P,Hu S,et al.Simultaneous determination of oxygen,nitrogen and hydrogen in metals by pulse heating and time of flight mass spectrometric method[J].Talanta.2011,84(4):1057-1062.
[71]马爱方.火花源发射光谱仪测定钢中的氧[J].河北冶金(Hebei Metallurgy),2003(6):53-55.
[72]刘辉,张春晓,胡军,等.火花源原子发射光谱法测定NiFeCr合金中氮[J].冶金分析(Metallurgical Analysis),2012,32(6):10-13.
[73]Laur F,Carolina D A.阿塞洛米塔尔图巴朗钢铁集团火花发射光谱法优化氮的分析[J].冶金分析(Metallurgical Analysis),2012,32(7):25-31.