氧化锆制备技术的研究现状与进展
|
摘要
对几种常见的氧化锆制备技术进行了介绍,并分析了这些技术的优势。化学法制备的氧化锆粒径分布均匀且该方法简单易行。溶胶-凝胶法制备的氧化锆粒径小、单分散性能优异。水热法制备的氧化锆粒径小、纯度高。电熔法制备的氧化锆杂质含量低,致密度高且制备工艺简单。微波热处理制备的氧化锆反应时间短、升温速率快、能耗小。氧化锆的多种制备工艺技术使得其性能及应用更加的多样化。
Several common zirconia preparation techniques were introduced and their advantages were analyzed.The particle size distribution of zirconia prepared by chemical method is uniform and the method is simple and convenient.The zirconia prepared by Sol-Gel method has small particle size and excellent monodisperse properties.The zirconia prepared by hydrothermal method has small particle size and high purity.The zirconia prepared by electrofusion method has low impurity content,high density and simple production process.The zirconia prepared by microwave heat treatment has the advantages of short reaction time,fast heating rate and low energy consumption.The properties and applications of zirconia are more diversified due to its various preparation technologies.
Several common zirconia preparation techniques were introduced and their advantages were analyzed.The particle size distribution of zirconia prepared by chemical method is uniform and the method is simple and convenient.The zirconia prepared by Sol-Gel method has small particle size and excellent monodisperse properties.The zirconia prepared by hydrothermal method has small particle size and high purity.The zirconia prepared by electrofusion method has low impurity content,high density and simple production process.The zirconia prepared by microwave heat treatment has the advantages of short reaction time,fast heating rate and low energy consumption.The properties and applications of zirconia are more diversified due to its various preparation technologies.
引文
[1]熊炳昆.二氧化锆制备工艺与应用[M].北京:冶金工业出版社,2008.
[2]巫兰萍,费文宗.氧化锆性质及其应用前景概述[J].四川化工,2013,16(1):25-27.
[3]余鑫萌,徐宝奎,袁发得.二氧化锆的稳定化及其应用[J].中国材料进展,2007,26(1):28-32.
[4]郭宝贵,云峰,安胜利.反相微乳液碳吸附耦合法制备氧化钇稳定四方氧化锆纳米粉体及表征[J].稀土,2010,31(1):57-60.
[5]郭宝贵,云峰,安胜利.碳吸附沉淀法制备氧化钇稳定氧化锆纳米粉末研究[J],粉末冶金技术,2009,27(4):247-250.
[6]马中义,徐润,杨成,等.不同形态ZrO2的制备及其表面性质研究[J].物理化学学报,2004,20(10):1221-1225.
[7]吴刚强,徐绍平,王煜炎,等.载体用高比表面超细二氧锆的制备及结构表征[J].无机盐工业,2017,49(10):26-29.
[8]蒋东民,王力军,车小奎.氧氯化锆制备工艺与应用[M].北京:冶金工业出版社,2012.
[9]宋艳玲,周迎春,张启俭.溶胶-凝胶法制备纳米二氧化锆[J].辽宁化工,2004,33(12):688-690.
[10]徐黎岭,崔硕,吴立昂,等.溶胶-凝胶法制备氧化锆粉体[J].稀有金属材料与工程,2010(增刊2):506-508.
[11]AND S S,SEAL S.Thermodynamic tetragonal phase stability in Sol-Gel derived nanodomains of pure zirconia[J].Journal of Physical Chemistry B,2016,108(11):3395-3399.
[12]BOULOS L,FORUZANMEHR M R,TAGNIT-HAMOU A,et al.Wetting analysis and surface characterization of flax fibers modified with zirconia by sol-gel method[J].Surface&Coatings Technology,2017,313:407-416.
[13]同帜,霍乐乐,董旭娟,等.溶胶-凝胶法制备氧化锆薄膜的工艺与表征[J].粉末冶金材料科学与工程,2016,21(1):174-179.
[14]赵志龙,薛群虎,丁冬海,等.溶胶-凝胶法制备ZrO2粉的工艺研究[J].耐火材料,2017,51(6):422-425.
[15]杨连弟,张文丽,侯贵芹.水热法制备纳米氧化锆粉体[J].河北联合大学学报(自然科学版),2010,32(2):50-52.
[16]代文双,杨煜.水热法制备氧化锆超细粉体工艺研究[J].辽宁科技学院学报,2016,18(3):1-2.
[17]MURASE Y,KATO E.Preparation of Zirconia Whiskers from Zirconium Hydroxide in Sulfuric Acid Solutions under Hydrothermal Conditions at 200℃[J].Journal of the American Ceramic Society,2010,84(11):2705-2706.
[18]梁新杰,仇越秀,王洪友,等.水热-水解法制备氧化锆粉体及其表征[J].材料导报,2015,29(2):43-46.
[19]包晓刚,叶旦旺,胡天喜,等.一种高纯度电熔氧化锆:CN105905942A[P].2016-08-31.
[20]田丰.电熔氧化锆粉体的制备与性能研究[D].杭州:浙江大学,2012.
[21]GUO S,CHEN G,PENG J,et al.Preparation of partially stabilized zirconia from fused zirconia using roasting[J].Journal of Alloys&Compounds,2010,506(1):L5-L7.
[22]齐凤元,毕海燕,邵悦.用电熔氧化锆制备氧氯化锆的实验研究[J].稀有金属与硬质合金,2017(5):50-52.
[23]郭胜惠,陈菓,彭金辉,等.微波加热处理电熔ZrO2制备部分稳定ZrO2[J].耐火材料,2008,42(5):372-374.
[24]MAZAHERI M,ZAHEDI A M,HEJAZI M M.Processing of nanocrystalline 8 mol%yttria-stabilized zirconia by conventional,microwave-assisted and twostep sintering[J].Materials Science and Engineering:A,2008,492(1):261-267.
[25]李静,彭金辉,郭胜惠,等.采用天然斜锆石微波烧结制备部分稳定氧化锆陶瓷[J].钛工业进展,2011,28(3):14-16.
[26]刘扬帆.微波干燥热解制备纳米ZrO2粉体及其性能研究[D].郑州:郑州航空工业管理学院,2017.
[27]郭胜惠,彭金辉,陈菓,等.电熔氧化锆在微波场中的吸波特性和升温行为[J].中南大学学报(自然科学版),2009(4):915-920.
[2]巫兰萍,费文宗.氧化锆性质及其应用前景概述[J].四川化工,2013,16(1):25-27.
[3]余鑫萌,徐宝奎,袁发得.二氧化锆的稳定化及其应用[J].中国材料进展,2007,26(1):28-32.
[4]郭宝贵,云峰,安胜利.反相微乳液碳吸附耦合法制备氧化钇稳定四方氧化锆纳米粉体及表征[J].稀土,2010,31(1):57-60.
[5]郭宝贵,云峰,安胜利.碳吸附沉淀法制备氧化钇稳定氧化锆纳米粉末研究[J],粉末冶金技术,2009,27(4):247-250.
[6]马中义,徐润,杨成,等.不同形态ZrO2的制备及其表面性质研究[J].物理化学学报,2004,20(10):1221-1225.
[7]吴刚强,徐绍平,王煜炎,等.载体用高比表面超细二氧锆的制备及结构表征[J].无机盐工业,2017,49(10):26-29.
[8]蒋东民,王力军,车小奎.氧氯化锆制备工艺与应用[M].北京:冶金工业出版社,2012.
[9]宋艳玲,周迎春,张启俭.溶胶-凝胶法制备纳米二氧化锆[J].辽宁化工,2004,33(12):688-690.
[10]徐黎岭,崔硕,吴立昂,等.溶胶-凝胶法制备氧化锆粉体[J].稀有金属材料与工程,2010(增刊2):506-508.
[11]AND S S,SEAL S.Thermodynamic tetragonal phase stability in Sol-Gel derived nanodomains of pure zirconia[J].Journal of Physical Chemistry B,2016,108(11):3395-3399.
[12]BOULOS L,FORUZANMEHR M R,TAGNIT-HAMOU A,et al.Wetting analysis and surface characterization of flax fibers modified with zirconia by sol-gel method[J].Surface&Coatings Technology,2017,313:407-416.
[13]同帜,霍乐乐,董旭娟,等.溶胶-凝胶法制备氧化锆薄膜的工艺与表征[J].粉末冶金材料科学与工程,2016,21(1):174-179.
[14]赵志龙,薛群虎,丁冬海,等.溶胶-凝胶法制备ZrO2粉的工艺研究[J].耐火材料,2017,51(6):422-425.
[15]杨连弟,张文丽,侯贵芹.水热法制备纳米氧化锆粉体[J].河北联合大学学报(自然科学版),2010,32(2):50-52.
[16]代文双,杨煜.水热法制备氧化锆超细粉体工艺研究[J].辽宁科技学院学报,2016,18(3):1-2.
[17]MURASE Y,KATO E.Preparation of Zirconia Whiskers from Zirconium Hydroxide in Sulfuric Acid Solutions under Hydrothermal Conditions at 200℃[J].Journal of the American Ceramic Society,2010,84(11):2705-2706.
[18]梁新杰,仇越秀,王洪友,等.水热-水解法制备氧化锆粉体及其表征[J].材料导报,2015,29(2):43-46.
[19]包晓刚,叶旦旺,胡天喜,等.一种高纯度电熔氧化锆:CN105905942A[P].2016-08-31.
[20]田丰.电熔氧化锆粉体的制备与性能研究[D].杭州:浙江大学,2012.
[21]GUO S,CHEN G,PENG J,et al.Preparation of partially stabilized zirconia from fused zirconia using roasting[J].Journal of Alloys&Compounds,2010,506(1):L5-L7.
[22]齐凤元,毕海燕,邵悦.用电熔氧化锆制备氧氯化锆的实验研究[J].稀有金属与硬质合金,2017(5):50-52.
[23]郭胜惠,陈菓,彭金辉,等.微波加热处理电熔ZrO2制备部分稳定ZrO2[J].耐火材料,2008,42(5):372-374.
[24]MAZAHERI M,ZAHEDI A M,HEJAZI M M.Processing of nanocrystalline 8 mol%yttria-stabilized zirconia by conventional,microwave-assisted and twostep sintering[J].Materials Science and Engineering:A,2008,492(1):261-267.
[25]李静,彭金辉,郭胜惠,等.采用天然斜锆石微波烧结制备部分稳定氧化锆陶瓷[J].钛工业进展,2011,28(3):14-16.
[26]刘扬帆.微波干燥热解制备纳米ZrO2粉体及其性能研究[D].郑州:郑州航空工业管理学院,2017.
[27]郭胜惠,彭金辉,陈菓,等.电熔氧化锆在微波场中的吸波特性和升温行为[J].中南大学学报(自然科学版),2009(4):915-920.