纳米镍粉的制备与应用的发展趋势
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摘要
介绍了等离子体法、液相还原法、电火花放电腐蚀法和高能球磨法等几种纳米镍粉的常见制备方法,总结了各种方法的优缺点,归纳了在纳米镍粉的制备过程中存在着难以实现规模化生产、纯度难以控制等问题;其研究趋势是通过分析其成核与生长机理,找到最佳合成条件以实现纳米镍粉的可控制备。另外,本文重点叙述了纳米镍粉在多层陶瓷电容器(MLCC)和催化剂等领域的应用现状,从应用的角度阐述了各个领域对纳米镍粉的需求。在纳米镍粉的应用中,存在着易氧化及同其他材料匹配性差等问题,需要通过表面改性等手段优化其应用性能。最后,文章指出将纳米镍粉的应用与其制备方法相结合,用最合适的方法制备出符合应用要求的纳米镍粉,是未来纳米镍粉的研究趋势。
This paper introduces the common preparation methods of nickel nano-powder such as the plasma, liquid phase reduction, spark discharge erosion and high energy ball milling. The advantages and disadvantages of these methods are summarized. There are however still several problems in the preparation of nickel nano-powder. For instance, it is difficult to achieve large-scale production and the purity and performance are difficult to meet the application requirements. The research trends are concluded as analyzing the nucleation and growth mechanism, and finding the best synthesis conditions to prepare the nickel nano-powder controllably. In addition, this paper describes the application status and demands of nickel nano-powder in MLCC and catalysts and points out that the problems of easy oxidation, poor matching with other materials need to be overcome. It is necessary to optimize its performance by surface modification or by other ways. At last, the research tendency of nickel nanopowder in the future are to bind the application of nickel nano-powder with its preparation method, that is using the most suitable preparation method to meets the application requirement.
This paper introduces the common preparation methods of nickel nano-powder such as the plasma, liquid phase reduction, spark discharge erosion and high energy ball milling. The advantages and disadvantages of these methods are summarized. There are however still several problems in the preparation of nickel nano-powder. For instance, it is difficult to achieve large-scale production and the purity and performance are difficult to meet the application requirements. The research trends are concluded as analyzing the nucleation and growth mechanism, and finding the best synthesis conditions to prepare the nickel nano-powder controllably. In addition, this paper describes the application status and demands of nickel nano-powder in MLCC and catalysts and points out that the problems of easy oxidation, poor matching with other materials need to be overcome. It is necessary to optimize its performance by surface modification or by other ways. At last, the research tendency of nickel nanopowder in the future are to bind the application of nickel nano-powder with its preparation method, that is using the most suitable preparation method to meets the application requirement.
引文
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[19]LIU Y,ZHU K,LI X,et al.Analysis of multi-scale Ni particles generated by ultrasonic aided electrical discharge erosion in pure water[J].Advanced Powder Technology,2018,29(4):863-873.
[20]ZHANG J,ZHANG C,LIU Z,et al.High-performance ball-milled SiOx,anodes for lithium ion batteries[J].Journal of Power Sources,2017,339:86-92.
[21]PANIGRAHI B B,DAS K,GODKHINDI M M.Dilatometry of ball milled nickel nano powder during non-isothermal sintering[J].Science of Sintering,2007,39(1):25-29.
[22]ZHAO Y,SHEN T D,ZHANG J.High P-T,nano-mechanics of polycrystalline nickel[J].Nanoscale Research Letters,2007,2(10):476-491.
[23]路承杰,张振忠,周剑秋,等.高能球磨法制备纳米晶Ni粉的研究[J].铸造技术,2007,28(6):775-778.LU C J,ZHANG Z Z,ZHOU J Q,et al.Preparation of nancrystalline nickel powders by high energy ball milling[J].Foundry Technology,2007,28(6):775-778.
[24]CAI Z,WANG X,LUO B,et al.Multiscale design of high-voltage multilayer energy-storage ceramic capacitors[J].Journal of the American Ceramic Society,2018,101(4):1607-1615.
[25]KISHI H,MIZUNO Y,CHAZONO H.Base-metal electrodemultilayer ceramic capacitors:past,present and future perspectives[J].Japanese Journal of Applied Physics,2003,42(1):1-15.
[26]WANG P,XU H,ZHU G,et al.An efficient method to achieve MLCCminiaturization and ensure its reliability[J].Journal of Materials Science Materials in Electronics,2016,28(5):1-5.
[27]JEON J,LEE H,PU B,et al.Prediction of impedance characteristics of MLCC using multiconductor transmission line theory[J].IEEETransactions on Electromagnetic Compatibility,2016,58(6):1760-1771.
[28]HIROSE S,USUI T,CROSSLEY S,et al.Progress on electrocaloric multilayer ceramic capacitor development[J].APL Materials,2016,4(6):27-43.
[29]WANG S H,CHAI Y L,LEE W H.A novel approach to sintering(Ba,Ca)(Ti,Zr)O3multilayer ceramic capacitors with Ni electrodes[J].Journal of the European Ceramic Society,2012,32(8):1711-1723.
[30]郭顺,王东新,李军义.MLCC用超细镍粉的制备方法及发展趋势[J].材料导报,2012,26(2):212-215.GUO S,WANG D X,LI J Y.Preparation methods and development tendency of ultrafine nickel powder used in MLCC[J].Materials Review,2012,26(2):212-215.
[31]GONG H,WANG X,TIAN Z,et al.Interfacial diffusion behavior in Ni-BaTiO3MLCCs with ultra-thin active layers[J].Electronic Materials Letters,2014,10(2):417-421.
[32]SADA T,FUJIKAWA N.Analysis of insulation resistance degradation in Ni-BaTiO3multilayer ceramic capacitors under highly accelerated life test[J].Japanese Journal of Applied Physics,2017,56(10):104-108.
[33]WANG P,XU H R,ZHU G S,et al.An efficient method to achieve MLCC miniaturization and ensure its reliability[J].Journal of Materials Science:Materials in Electronics,2016,28(5):1-5.
[34]SALEEM M,SONG J S,JEONG S J,et al.Dielectric response on microwave sintered BaTiO3,composite with Ni nanopowder and paste[J].Materials Research Bulletin,2015,64:380-385.
[35]DAS V,PADMANABAN S,VENKITUSAMY K,et al.Recent advances and challenges of fuel cell based power system architectures and control-A review[J].Renewable and Sustainable Energy Reviews,2017,73:10-18.
[36]AKHAIRI M A F,KAMARUDIN S K.Catalysts in direct ethanol fuel cell(DEFC):an overview[J].International Journal of Hydrogen Energy,2016,41(7):4214-4228.
[37]LAN R,TAO S.Preparation of nano-sized nickel as anode catalyst for direct urea and urine fuel cells[J].Journal of Power Sources,2011,196(11):5021-5026.
[38]KRISHNAMURTHY G,SHIVAKUMAR M S.Electroless deposition of nanosized nickel over graphite substrate with better coating coverage and catalytic activity for fuel cell application[J].Journal of Applied Electrochemistry,2017,47(4):519-529.
[39]GHASEMI M,WAN R W D,RAHIMNEJAD M,et al.Copperphthalocyanine and nickel nanoparticles as novel cathode catalysts in microbial fuel cells[J].International Journal of Hydrogen Energy,2013,38(22):9533-9540.
[40]REN Z,WU Z,SONG W,et al.Low temperature propane oxidation over Co3O4,based nano-array catalysts:Ni dopant effect,reaction mechanism and structural stability[J].Applied Catalysis B:Environmental,2016,180:150-160.
[41]KUMAR D,MANGALVEDEKAR H A,MAHAJAN S K.Nano-nickel catalytic dehydrogenation of ammonia borane[J].Materials for Renewable and Sustainable Energy,2014,3(2):23-30.
[42]WEI L I,ZHU J H,QI J H.Application of nano-nickel catalyst in the viscosity reduction of Liaohe extra-heavy oil by aqua-thermolysis[J].Journal of Fuel Chemistry and Technology,2007,35(2):176-180.
[43]WRONSKI Z S,CARPENTER G J C,CZUJKO T,et al.A new nanonickel catalyst for hydrogen storage in solid-state magnesium hydrides[J].International Journal of Hydrogen Energy,2011,36(1):1159-1166.
[44]TSAI T Y,LI Y A,SU H C,et al.Low temperature growth of carbon nanotubes using Ni nanopowder mixed with Ag-paste as catalyst[J].Diamond and Related Materials,2008,17(4):594-597.
[45]BAI Y,ZHANG J,YANG G,et al.Insight into the nanoparticle growth in supported Ni catalysts during the early stage of CO hydrogenation reaction:the important role of adsorbed CO molecules[J].ACSCatalysis,2018,8:6367-6374.
[46]KHORT A,PODBOLOTOV K,GARCíA R S,et al.One-step solution combustion synthesis of pure Ni nanopowders with enhanced coercivity:the fuel effect[J].Journal of Solid State Chemistry,2017,253:270-276.
[47]EWING S J,LAN R,XU X X,et al.Synthesis of dendritic nano-sized nickel for use as anode material in an alkaline membrane fuel cell[J].Fuel Cells,2010,10(1):72-76.
[48]LO C H,TSUNG T T,CHEN L C.Ni Nano-magnetic fluid prepared by submerged arc nano synthesis system(SANSS)[J].Jsme International Journal,2005,48(4):750-755.
[49]GAO R,JIANG Y,ABDELAZIZ S.All-fiber magnetic field sensors based on magnetic fluid-filled photonic crystal fibers[J].Optics Letters,2013,38(9):1539-1541.
[50]JIANG Z,LI S F,ZHAO F Q,et al.Research on the combustion properties of propellants with low content of nano metal powders[J].Propellants Explosives Pyrotechnics,2010,31(2):139-147.
[51]BROSTOW W,BROZYNSKI M,DATASHVILI T,et al.Strong thermoplastic elastomers created using nickel nanopowder[J].Polymer Bulletin,2011,67(8):1671-1696.
[52]GAIN A K,CHAN Y C,YUNG W K C.Effect of nano Ni additions on the structure and properties of Sn-9Zn and Sn-Zn-3Bi solders in Au/Ni/Cu ball grid array packages[J].Materials Science and Engineering B,2009,162(2):92-98.
[53]QI H P,CAO H L,HUANG Y D.Synthesis of flowerlike nickel particles and their microwave absorbing properties[J].Journal of Central South University,2014,21(8):3007-3012.
[54]PARVEEN S,MISRA R,SAHOO S K.Nanoparticles:a boon to drug delivery,therapeutics,diagnostics and imaging[J].Nanomedicine Nanotechnology Biology and Medicine,2012,8(2):147-166.
[55]郝晓光.多层陶瓷电容器用镍内电极浆料的现状与展望[J].电子元件与材料,2017,36(2):1-5.HAO X G.Current situation and development prospect of nickel inner electrode paste used in MLCC[J].Electronic Components and Materials,2017,36(2):1-5.
[2]ARAKHA M,JHA S.Synthesis and characterization of nanoparticles[J].Journal of Magnetism and Magnetic Materials,2018,322(8):1015-1019.
[3]FLAURAUD V,MASTRANGELI M,BERNASCONI G D,et al.Nanoscale topographical control of capillary assembly of nanoparticles[J].Nature Nanotechnology,2017,12(1):73-80.
[4]GONZALEZ I,JESUS D,CANIZALES E,et al.Comparison of the surface state of Ni nanoparticles used for methane catalytic decomposition[J].Journal of Physical Chemistry C,2016,116(40):21577-21587.
[5]WANG C,ZHANG X M,QIAN X F,et al.Preparation of nanocrystalline nickel powders through hydrothermal-reduction method[J].Materials Research Bulletin,1998,33(12):1747-1751.
[6]NAMDEO M,SAXENA S,TANKHIWALE R,et al.Magnetic nanoparticles for drug delivery applications[J].Journal of Nanoscience and Nanotechnology,2017,8(7):3247-3271.
[7]ZHANG H,ZOU G,LIU L,et al.Synthesis of silver nanoparticles using large-area arc discharge and its application in electronic packaging[J].Journal of Materials Science,2017,52(6):3375-3387.
[8]GERSHMAN S,RAITSES Y.Unstable behavior of anodic arc discharge for synthesis of nanomaterials[J].Journal of Physics D:Applied Physics,2016,49(34):345201-345222.
[9]WEI Z,XIA T,BAI L,et al.Efficient preparation for Ni nanopowders by anodic arc plasma[J].Materials Letters,2006,60(6):766-770.
[10]CHO Y S,MOON J W,CHUNG K C,et al.Synthesis of nickel and copper nanopowders by plasma arc evaporation[J].Journal of Korean Powder Metallurgy Institute,2013,20(6):411-424.
[11]LIANG F,TANAKA M,CHOI S,et al.Investigation of the relationship between arc-anode attachment mode and anode temperature for nickel nanoparticle production by a DC arc discharge[J].Journal of Physics D:Applied Physics,2016,49(12):125201-125217.
[12]BAI L,FAN J,PENG H,et al.RF plasma synthesis of nickel nanopowders via hydrogen reduction of nickel hydroxide/carbonate[J].Journal of Alloys and Compounds,2009,481(1):563-567.
[13]CHAU J L H.Synthesis of Ni and bimetallic FeNi nanopowders by microwave plasma method[J].Materials Letters,2007,61(13):2753-2756.
[14]ABDEL-AAL E A,MALEKZADEH S M,RASHAD M M,et al.Effect of synthesis conditions on preparation of nickel metal nanopowders via hydrothermal reduction technique[J].Powder Technology,2007,171(1):63-68.
[15]YU Y,MA H,TIAN X X,et al.Synthesis and electromagnetic absorption properties of micro-nano nickel powders prepared with liquid phase reduction method[J].Journal of Advanced Dielectrics,2016,6(3):1650025-1650032.
[16]TIENTONG J,GARCIA S,THURBER C,et al.Synthesis of nickel and nickel hydroxide nanopowders by simplified chemical reduction[J].Journal of Nanotechnology,2014(4):1-6.
[17]TSENG K H,CHUNG M Y,CHIU J L.Suspension stability of nanoAu and nano-Ag colloids prepared by electrical spark discharge method[J].Journal of Cluster Science,2017,28(100):1-16.
[18]李忠丽,李翔龙,文玉华,等.电火花腐蚀制备Ni粉[J].微细加工技术,2007,2(2):57-59.LI Z L,LI X L,WEN Y H,et al.Preparation of nickel powder by spark-eroded method[J].Microfabrication Technology,2007,2(2):57-59.
[19]LIU Y,ZHU K,LI X,et al.Analysis of multi-scale Ni particles generated by ultrasonic aided electrical discharge erosion in pure water[J].Advanced Powder Technology,2018,29(4):863-873.
[20]ZHANG J,ZHANG C,LIU Z,et al.High-performance ball-milled SiOx,anodes for lithium ion batteries[J].Journal of Power Sources,2017,339:86-92.
[21]PANIGRAHI B B,DAS K,GODKHINDI M M.Dilatometry of ball milled nickel nano powder during non-isothermal sintering[J].Science of Sintering,2007,39(1):25-29.
[22]ZHAO Y,SHEN T D,ZHANG J.High P-T,nano-mechanics of polycrystalline nickel[J].Nanoscale Research Letters,2007,2(10):476-491.
[23]路承杰,张振忠,周剑秋,等.高能球磨法制备纳米晶Ni粉的研究[J].铸造技术,2007,28(6):775-778.LU C J,ZHANG Z Z,ZHOU J Q,et al.Preparation of nancrystalline nickel powders by high energy ball milling[J].Foundry Technology,2007,28(6):775-778.
[24]CAI Z,WANG X,LUO B,et al.Multiscale design of high-voltage multilayer energy-storage ceramic capacitors[J].Journal of the American Ceramic Society,2018,101(4):1607-1615.
[25]KISHI H,MIZUNO Y,CHAZONO H.Base-metal electrodemultilayer ceramic capacitors:past,present and future perspectives[J].Japanese Journal of Applied Physics,2003,42(1):1-15.
[26]WANG P,XU H,ZHU G,et al.An efficient method to achieve MLCCminiaturization and ensure its reliability[J].Journal of Materials Science Materials in Electronics,2016,28(5):1-5.
[27]JEON J,LEE H,PU B,et al.Prediction of impedance characteristics of MLCC using multiconductor transmission line theory[J].IEEETransactions on Electromagnetic Compatibility,2016,58(6):1760-1771.
[28]HIROSE S,USUI T,CROSSLEY S,et al.Progress on electrocaloric multilayer ceramic capacitor development[J].APL Materials,2016,4(6):27-43.
[29]WANG S H,CHAI Y L,LEE W H.A novel approach to sintering(Ba,Ca)(Ti,Zr)O3multilayer ceramic capacitors with Ni electrodes[J].Journal of the European Ceramic Society,2012,32(8):1711-1723.
[30]郭顺,王东新,李军义.MLCC用超细镍粉的制备方法及发展趋势[J].材料导报,2012,26(2):212-215.GUO S,WANG D X,LI J Y.Preparation methods and development tendency of ultrafine nickel powder used in MLCC[J].Materials Review,2012,26(2):212-215.
[31]GONG H,WANG X,TIAN Z,et al.Interfacial diffusion behavior in Ni-BaTiO3MLCCs with ultra-thin active layers[J].Electronic Materials Letters,2014,10(2):417-421.
[32]SADA T,FUJIKAWA N.Analysis of insulation resistance degradation in Ni-BaTiO3multilayer ceramic capacitors under highly accelerated life test[J].Japanese Journal of Applied Physics,2017,56(10):104-108.
[33]WANG P,XU H R,ZHU G S,et al.An efficient method to achieve MLCC miniaturization and ensure its reliability[J].Journal of Materials Science:Materials in Electronics,2016,28(5):1-5.
[34]SALEEM M,SONG J S,JEONG S J,et al.Dielectric response on microwave sintered BaTiO3,composite with Ni nanopowder and paste[J].Materials Research Bulletin,2015,64:380-385.
[35]DAS V,PADMANABAN S,VENKITUSAMY K,et al.Recent advances and challenges of fuel cell based power system architectures and control-A review[J].Renewable and Sustainable Energy Reviews,2017,73:10-18.
[36]AKHAIRI M A F,KAMARUDIN S K.Catalysts in direct ethanol fuel cell(DEFC):an overview[J].International Journal of Hydrogen Energy,2016,41(7):4214-4228.
[37]LAN R,TAO S.Preparation of nano-sized nickel as anode catalyst for direct urea and urine fuel cells[J].Journal of Power Sources,2011,196(11):5021-5026.
[38]KRISHNAMURTHY G,SHIVAKUMAR M S.Electroless deposition of nanosized nickel over graphite substrate with better coating coverage and catalytic activity for fuel cell application[J].Journal of Applied Electrochemistry,2017,47(4):519-529.
[39]GHASEMI M,WAN R W D,RAHIMNEJAD M,et al.Copperphthalocyanine and nickel nanoparticles as novel cathode catalysts in microbial fuel cells[J].International Journal of Hydrogen Energy,2013,38(22):9533-9540.
[40]REN Z,WU Z,SONG W,et al.Low temperature propane oxidation over Co3O4,based nano-array catalysts:Ni dopant effect,reaction mechanism and structural stability[J].Applied Catalysis B:Environmental,2016,180:150-160.
[41]KUMAR D,MANGALVEDEKAR H A,MAHAJAN S K.Nano-nickel catalytic dehydrogenation of ammonia borane[J].Materials for Renewable and Sustainable Energy,2014,3(2):23-30.
[42]WEI L I,ZHU J H,QI J H.Application of nano-nickel catalyst in the viscosity reduction of Liaohe extra-heavy oil by aqua-thermolysis[J].Journal of Fuel Chemistry and Technology,2007,35(2):176-180.
[43]WRONSKI Z S,CARPENTER G J C,CZUJKO T,et al.A new nanonickel catalyst for hydrogen storage in solid-state magnesium hydrides[J].International Journal of Hydrogen Energy,2011,36(1):1159-1166.
[44]TSAI T Y,LI Y A,SU H C,et al.Low temperature growth of carbon nanotubes using Ni nanopowder mixed with Ag-paste as catalyst[J].Diamond and Related Materials,2008,17(4):594-597.
[45]BAI Y,ZHANG J,YANG G,et al.Insight into the nanoparticle growth in supported Ni catalysts during the early stage of CO hydrogenation reaction:the important role of adsorbed CO molecules[J].ACSCatalysis,2018,8:6367-6374.
[46]KHORT A,PODBOLOTOV K,GARCíA R S,et al.One-step solution combustion synthesis of pure Ni nanopowders with enhanced coercivity:the fuel effect[J].Journal of Solid State Chemistry,2017,253:270-276.
[47]EWING S J,LAN R,XU X X,et al.Synthesis of dendritic nano-sized nickel for use as anode material in an alkaline membrane fuel cell[J].Fuel Cells,2010,10(1):72-76.
[48]LO C H,TSUNG T T,CHEN L C.Ni Nano-magnetic fluid prepared by submerged arc nano synthesis system(SANSS)[J].Jsme International Journal,2005,48(4):750-755.
[49]GAO R,JIANG Y,ABDELAZIZ S.All-fiber magnetic field sensors based on magnetic fluid-filled photonic crystal fibers[J].Optics Letters,2013,38(9):1539-1541.
[50]JIANG Z,LI S F,ZHAO F Q,et al.Research on the combustion properties of propellants with low content of nano metal powders[J].Propellants Explosives Pyrotechnics,2010,31(2):139-147.
[51]BROSTOW W,BROZYNSKI M,DATASHVILI T,et al.Strong thermoplastic elastomers created using nickel nanopowder[J].Polymer Bulletin,2011,67(8):1671-1696.
[52]GAIN A K,CHAN Y C,YUNG W K C.Effect of nano Ni additions on the structure and properties of Sn-9Zn and Sn-Zn-3Bi solders in Au/Ni/Cu ball grid array packages[J].Materials Science and Engineering B,2009,162(2):92-98.
[53]QI H P,CAO H L,HUANG Y D.Synthesis of flowerlike nickel particles and their microwave absorbing properties[J].Journal of Central South University,2014,21(8):3007-3012.
[54]PARVEEN S,MISRA R,SAHOO S K.Nanoparticles:a boon to drug delivery,therapeutics,diagnostics and imaging[J].Nanomedicine Nanotechnology Biology and Medicine,2012,8(2):147-166.
[55]郝晓光.多层陶瓷电容器用镍内电极浆料的现状与展望[J].电子元件与材料,2017,36(2):1-5.HAO X G.Current situation and development prospect of nickel inner electrode paste used in MLCC[J].Electronic Components and Materials,2017,36(2):1-5.
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