快速溶剂萃取技术在农兽药残留检测中的应用与展望
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摘要
在针对复杂基质样品中,农兽药残留的检测中前处理技术是样品分析过程中关键的一步。加速溶剂萃取技术具有操作简便,使用溶剂少、提取效率高、萃取操作完全自动化等特点,已广泛应用于食品、环境等分析领域。本文阐述了快速溶剂萃取技术的基本原理,综述了近几年快速溶剂萃取技术在农兽药残留检测中的应用,并对其发展的前景进行了展望。
In the determination of pesticide residues and veterinary drug residues in the complicated matrix samples,the pretreatment technique is very important.Accelerated solvent extraction(ASE) had been widely used in food,environment and other fields because of its advantages of easy to operate,less solvent,high-efficient extraction and automatic in the extraction procedures.In this paper,the basic theory of ASE was introduced,and the applications of ASE on the analysis of pesticide residues and veterinary drug residues were summarized.Furthermore,the development prospect of ASE was also introduced.
In the determination of pesticide residues and veterinary drug residues in the complicated matrix samples,the pretreatment technique is very important.Accelerated solvent extraction(ASE) had been widely used in food,environment and other fields because of its advantages of easy to operate,less solvent,high-efficient extraction and automatic in the extraction procedures.In this paper,the basic theory of ASE was introduced,and the applications of ASE on the analysis of pesticide residues and veterinary drug residues were summarized.Furthermore,the development prospect of ASE was also introduced.
引文
[1] 赛默飞世尔科技.ASE快速溶剂萃取仪提取持久性有机污染物(POPs)的应用(一)[J].环境化学,2012,31(1):130-131.
[2] Wang Pu,Zhang Qinghua,Wang yawei,et al.Evaluation of Soxhlet extraction,accelerated solvent extraction and microwave-assisted extraction for the determination of polychlorinated biphenyls and polybrominated diphenyl ethers in soil and fish samples[J].Analytica Chimica Acta,2010,663(1):43-48.
[3] Supradip Saha,Suresh Walia,Aditi Kundu,et al.Optimal extraction and fingerprinting of carotenoids by accelerated solvent extraction and liquid chromatography with tandem mass spectrometry[J].Food Chemistry,2015,177(6):369-375.
[4] 计艺达.快速溶剂萃取技术(ASE)在水环境监测中的比较研究及展望[J].北方环境,2013,25(10):69-70.
[5] Popp P,Keil P,Moder M,et al.Application of accelerated solvent extraction followed by gas chromatography,high-performance liquid chromatography and gas chromatography-mass spectrometry for the determination of polycyclic aromatic hydrocarbons,chlorinated pesticides and polychlorinated dibenzo-p-dioxins and dibenzofurans in solid wastes [J].J Chromatogr A,1997,774(1):203-211.
[6] Heo Jiyoung,Suna Kim,Kang Jaehyun,et al.Determination of lutein from green tea and green tea by-products using accelerated solvent extraction and UPLC [J].Journal of Food Science,2014,79 (5):816-821.
[7] 章剑扬,刘新,车金水,等.快速溶剂萃取-离子色谱法测定茶叶中的有机酸[J].化学分析计量,2012,21(1):43-45.
[8] 刘静.ASE快速溶剂萃取-解决固体、半固体样品前处理的新技术[J].现代科学仪器,2002(3):59-61.
[9] 祝子铜.快速溶剂萃取-超高效液相色谱-串联质谱法测定蜂花粉中氯霉素[J].食品工业科技,2015,36(20):68-76.
[10] Lucia Mainero Rocca,Alessandra Gentili,Virginia Pérez-Fernández,et al.Veterinary drugs residues: a review of the latest analytical research on sample preparation and LC-MS based methods [J].Food Additives & Contaminants: Part A,34(5):766-784.
[11] 欧阳运富,唐宏兵,吴英,等.加速溶剂萃取-在线凝胶渗透色谱-气相色谱-质谱联用法快速测定蔬菜和水果中多农药残留[J].色谱,2012,30(7):654-659.
[12] 赵粼,阙斐,刘绿叶.快速溶剂萃取-超高效液相色谱法分析鱼肉中喹乙醇[J].分析试验室,2012,31(2):10-12.
[13] 于辉,赵萍.快速溶剂萃取-高效液相色谱-紫外串联荧光检测方法测定太平湖白鱼中4种氟喹诺酮类药物残留[J].中国食品卫生杂志, 2011,23(4):322-325.
[14] 陈舰,张景华.快速溶剂萃取-高效液相法测定茶叶中多菌灵残留量[J].广东化工,2011,38(1):170-172.
[15] 吴凤琪,聂冬锐,沈金灿,等.快速溶剂萃取在线凝胶渗透色谱-串联气质联用法测定大豆中53种农药残留量[J].食品安全质量检测学报,2014(11):3410-3417.
[16] 徐豪,徐龙山,钱家亮,等.快速溶剂萃取-凝胶渗透色谱净化-气相色谱-串联质谱分析猪肉中109种农药残留[J].食品安全质量检测学报,2016,7(6):2386-2395.
[17] 纪律,徐峻卿,李启,等.快速溶剂萃取-超高效液相色谱串联质谱法测定竹笋中的百草枯残留[J].中国卫生检验杂志,2018,28(1):18-21.
[18] 曹亚林,李伟,裴晓华,等.快速溶剂萃取-气相色谱法快速测定茶叶中7种拟除虫菊酯农残[J].分析仪器,2018(3):57-62.
[19] 安强,王伟,柳育良.QSE-HPLC快速测定动物源食品中硝基呋喃代谢产物[J].广东科技,2009,223:43-44.
[20] 于辉,游辉,武彦文,等.快速溶剂萃取-高下液相色谱法测定鸡肉中磺胺类药物残留[J].现代科学仪器,2010(6):93-96.
[21] 游辉,于辉,武彦文,等.快速溶剂萃取-基质固相分散-高效液相色谱法测定牛肉中5种磺胺类药物残留[J].分析测试学报,2010,29(10):1087-1090.
[22] 杨洪生,孟勇,张美琴,等.快速溶剂萃取-超高效液相色谱-串联质谱法同时测定水产品中氯霉素和氟苯尼考[J].理化检验-化学分册,2012,48(11):1353-1356.
[23] 饶桂维,李成平,王倩,等.快速溶剂萃取-高效液相色谱法测定禽蛋中磺胺嘧啶[J].化学分析计量,2017,26(1):20-23.
[2] Wang Pu,Zhang Qinghua,Wang yawei,et al.Evaluation of Soxhlet extraction,accelerated solvent extraction and microwave-assisted extraction for the determination of polychlorinated biphenyls and polybrominated diphenyl ethers in soil and fish samples[J].Analytica Chimica Acta,2010,663(1):43-48.
[3] Supradip Saha,Suresh Walia,Aditi Kundu,et al.Optimal extraction and fingerprinting of carotenoids by accelerated solvent extraction and liquid chromatography with tandem mass spectrometry[J].Food Chemistry,2015,177(6):369-375.
[4] 计艺达.快速溶剂萃取技术(ASE)在水环境监测中的比较研究及展望[J].北方环境,2013,25(10):69-70.
[5] Popp P,Keil P,Moder M,et al.Application of accelerated solvent extraction followed by gas chromatography,high-performance liquid chromatography and gas chromatography-mass spectrometry for the determination of polycyclic aromatic hydrocarbons,chlorinated pesticides and polychlorinated dibenzo-p-dioxins and dibenzofurans in solid wastes [J].J Chromatogr A,1997,774(1):203-211.
[6] Heo Jiyoung,Suna Kim,Kang Jaehyun,et al.Determination of lutein from green tea and green tea by-products using accelerated solvent extraction and UPLC [J].Journal of Food Science,2014,79 (5):816-821.
[7] 章剑扬,刘新,车金水,等.快速溶剂萃取-离子色谱法测定茶叶中的有机酸[J].化学分析计量,2012,21(1):43-45.
[8] 刘静.ASE快速溶剂萃取-解决固体、半固体样品前处理的新技术[J].现代科学仪器,2002(3):59-61.
[9] 祝子铜.快速溶剂萃取-超高效液相色谱-串联质谱法测定蜂花粉中氯霉素[J].食品工业科技,2015,36(20):68-76.
[10] Lucia Mainero Rocca,Alessandra Gentili,Virginia Pérez-Fernández,et al.Veterinary drugs residues: a review of the latest analytical research on sample preparation and LC-MS based methods [J].Food Additives & Contaminants: Part A,34(5):766-784.
[11] 欧阳运富,唐宏兵,吴英,等.加速溶剂萃取-在线凝胶渗透色谱-气相色谱-质谱联用法快速测定蔬菜和水果中多农药残留[J].色谱,2012,30(7):654-659.
[12] 赵粼,阙斐,刘绿叶.快速溶剂萃取-超高效液相色谱法分析鱼肉中喹乙醇[J].分析试验室,2012,31(2):10-12.
[13] 于辉,赵萍.快速溶剂萃取-高效液相色谱-紫外串联荧光检测方法测定太平湖白鱼中4种氟喹诺酮类药物残留[J].中国食品卫生杂志, 2011,23(4):322-325.
[14] 陈舰,张景华.快速溶剂萃取-高效液相法测定茶叶中多菌灵残留量[J].广东化工,2011,38(1):170-172.
[15] 吴凤琪,聂冬锐,沈金灿,等.快速溶剂萃取在线凝胶渗透色谱-串联气质联用法测定大豆中53种农药残留量[J].食品安全质量检测学报,2014(11):3410-3417.
[16] 徐豪,徐龙山,钱家亮,等.快速溶剂萃取-凝胶渗透色谱净化-气相色谱-串联质谱分析猪肉中109种农药残留[J].食品安全质量检测学报,2016,7(6):2386-2395.
[17] 纪律,徐峻卿,李启,等.快速溶剂萃取-超高效液相色谱串联质谱法测定竹笋中的百草枯残留[J].中国卫生检验杂志,2018,28(1):18-21.
[18] 曹亚林,李伟,裴晓华,等.快速溶剂萃取-气相色谱法快速测定茶叶中7种拟除虫菊酯农残[J].分析仪器,2018(3):57-62.
[19] 安强,王伟,柳育良.QSE-HPLC快速测定动物源食品中硝基呋喃代谢产物[J].广东科技,2009,223:43-44.
[20] 于辉,游辉,武彦文,等.快速溶剂萃取-高下液相色谱法测定鸡肉中磺胺类药物残留[J].现代科学仪器,2010(6):93-96.
[21] 游辉,于辉,武彦文,等.快速溶剂萃取-基质固相分散-高效液相色谱法测定牛肉中5种磺胺类药物残留[J].分析测试学报,2010,29(10):1087-1090.
[22] 杨洪生,孟勇,张美琴,等.快速溶剂萃取-超高效液相色谱-串联质谱法同时测定水产品中氯霉素和氟苯尼考[J].理化检验-化学分册,2012,48(11):1353-1356.
[23] 饶桂维,李成平,王倩,等.快速溶剂萃取-高效液相色谱法测定禽蛋中磺胺嘧啶[J].化学分析计量,2017,26(1):20-23.
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