甘肃省白银地区地骷髅水分、浸出物的质量研究
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摘要
目的:测定甘肃省白银地区地骷髅药材的水分和浸出物,为建立甘肃省地骷髅药材水分和浸出物的质量标准奠定基础。方法:参照《中国药典》2015年版四部通则方法,对甘肃省白银地区地骷髅药材的水分进行测定同时对其浸出物的提取条件进行优化。结果:以热水为提取溶剂测定地骷髅药材浸出物时含量最高,实验效果最理想。结论:确定地骷髅药材浸出物提取方法为药典通则热浸法(水为溶剂)。
Objective:To determine the water content and extract of the medicinal materials of Old Radish Root, and establish the quality standard of the water content and extract of Old Radish Root. Methods:According to the general principles of 《The Chinese Pharmacopoeia》(2015 edition), the water content of Old Radish Root medicinal materials was determined and the extraction conditions of its extracts were optimized. Results:Using hot water as extracting solvent to determine the extract of Old Radish Root medicinal materials, the content of the extract is the highest and the experimental effect is the best. Conclusions:The extraction method of the extract of Old Radish Root medicinal materials was determined to be the general rule of the Pharmacopoeia hot soaking method(water as solvent).
Objective:To determine the water content and extract of the medicinal materials of Old Radish Root, and establish the quality standard of the water content and extract of Old Radish Root. Methods:According to the general principles of 《The Chinese Pharmacopoeia》(2015 edition), the water content of Old Radish Root medicinal materials was determined and the extraction conditions of its extracts were optimized. Results:Using hot water as extracting solvent to determine the extract of Old Radish Root medicinal materials, the content of the extract is the highest and the experimental effect is the best. Conclusions:The extraction method of the extract of Old Radish Root medicinal materials was determined to be the general rule of the Pharmacopoeia hot soaking method(water as solvent).
引文
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[4]张璐.地骷髅药材的生药学鉴别研究[J].海峡药学,2017,29(1):32-34.
[5]《中国药典》2015年版四部(通则0832第二法)水分测定法.
[6]《中国药典》2015年版四部(通则2201)浸出物测定法.
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[8]郭彩杰,崔娜,李健,等.十字花科植物中莱菔硫烷防癌机制研究进展[J].西北植物学报,2009,26(10):2146-2152.
[9]吴华彰,费鸿君,黄银久,等.萝卜硫素的体外抗氧化和抑菌活性[J].中国老年学杂志,2012,2(32):750-753.
[2]吴晓彤.萝卜药用小便方[N].民族医药报,2002.
[3]张璐,房克慧.地骷髅药材薄层色谱鉴别研究[J].天津药学,2014,26(6):15-17.
[4]张璐.地骷髅药材的生药学鉴别研究[J].海峡药学,2017,29(1):32-34.
[5]《中国药典》2015年版四部(通则0832第二法)水分测定法.
[6]《中国药典》2015年版四部(通则2201)浸出物测定法.
[7]Poon T C,Hui A Y,Chan H L,et al.Prediction of liver fihrosis and cirrhosis in chronic hepatitis B infection by serum proteomic fingerprinting:a pilot study[J].Clin Chem,2005,51(2):328.
[8]郭彩杰,崔娜,李健,等.十字花科植物中莱菔硫烷防癌机制研究进展[J].西北植物学报,2009,26(10):2146-2152.
[9]吴华彰,费鸿君,黄银久,等.萝卜硫素的体外抗氧化和抑菌活性[J].中国老年学杂志,2012,2(32):750-753.