粮食加工品中玉米赤霉烯酮和呕吐毒素污染情况调查
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摘要
目的初步了解粮食加工品中玉米赤霉烯酮和呕吐毒素的污染情况。方法对北京地区和网购的200批次样品进行随机抽检,分别采用液相色谱法、免疫亲和层析净化高效液相色谱法对粮食加工品中的玉米赤霉烯酮和呕吐毒素进行了检测。结果初步调查发现玉米碾磨加工品中的玉米赤霉烯酮和小麦粉中的呕吐毒素检出率较高,分别达34%和74%;散装样品中玉米赤霉烯酮含量不合格率和检出率明显高于预包装样品。结论建议监管部门加强对散装玉米碾磨加工品和小麦粉等粮食加工品中毒素指标的监控力度和监测频次,同时针对我国特殊敏感人群加快设定合理限值。
Objective To investigate the contamination of zearalenone and deoxynivalenol in processed food.Methods A random sampling of 200 batches of samples from Beijing and online shopping was carried out, and zearalenone and deoxynivalenol in food processed products were detected by liquid chromatography, immunoaffinity chromatography and high performance liquid chromatography. Results Preliminary investigation showed that the detection rates of zearalenone in corn milling products and deoxynivalenol in wheat flour were higher(34% and 74%,respectively). The disqualification rate and detection rate of zearalenone in bulk samples were significantly higher than those in prepackaged samples. Conclusion It is recommended that the regulatory authorities strengthen the monitoring and monitoring frequency of toxins in food processed products such as bulk corn milled products and wheat flour, and speed up the setting of reasonable limits for special sensitive populations in China.
Objective To investigate the contamination of zearalenone and deoxynivalenol in processed food.Methods A random sampling of 200 batches of samples from Beijing and online shopping was carried out, and zearalenone and deoxynivalenol in food processed products were detected by liquid chromatography, immunoaffinity chromatography and high performance liquid chromatography. Results Preliminary investigation showed that the detection rates of zearalenone in corn milling products and deoxynivalenol in wheat flour were higher(34% and 74%,respectively). The disqualification rate and detection rate of zearalenone in bulk samples were significantly higher than those in prepackaged samples. Conclusion It is recommended that the regulatory authorities strengthen the monitoring and monitoring frequency of toxins in food processed products such as bulk corn milled products and wheat flour, and speed up the setting of reasonable limits for special sensitive populations in China.
引文
[1]胥革非.粮食发热与霉变[J].粮油储藏与检验,2001,1:30-38.Xu GF.Grain fever and mildew[J].J Grain Oil Stor Inspect,2001,1:30-38.
[2]Mishra HN,Chitrangada D.A review on biological control and metabolism of aflatoxin[J].Crit Rev Food Sci Nutr,2003,43:245-264.
[3]龚阿琼,罗金玲,胡骏鹏.2014年我国饲料原料中霉菌毒素含量的测定与分析[J].中国饲料,2015,(7):40-41.Gong AQ,Long JL,Hu JP.Detection and analysis of mycotoxin contamination of feed stuff in china in 2014[J].J Chin Feed,2015,(7):40-41.
[4]计成.霉菌毒素对家禽的危害及降解技术[J].中国家禽,2014,36(2):40-42.Ji C.The harm of mycotoxin to poultry and degradation technology[J].JChin Poul,2014,36(2):40-42.
[5]Mohamed EZ.Impact of mycotoxins on humans and animals[J].J Saud Chem Soc,2011,(15):129-144.
[6]王怡净,张立实.玉米赤霉烯酮毒性研究进展[J].中国食品卫生杂志.2002,14(5):41-43.Wang YJ,Zhang LS.Research progress of zearalenone toxicity[J].Chin JFood Hyg,2002,14(5):41-43.
[7]何庆华,许杨.玉米赤霉烯酮毒性研究及检测方法进展[J].卫生研究,2005,34(4):502-504.He QH,Xu Y.Advance in study on zearalenone’s toxicity and determination[J].J Hyg Res,2005,34(4):502-504.
[8]苗丽.常用饲料原料中玉米赤霉烯酮和呕吐毒素含量研究[D].泰安:山东农业大学,2015.Miao L.A field investigation of zearalenone and deoxynivalenol pollution in the common used feedstuffs[D].Taian:Shandong Agricultural University,2015.
[9]John CL,Josephine H,Irene P,et al.Workshopon Trichothecenes with a focus On DON:Sum-mary report[J].Toxicol Lett,2004,153:1-22.
[10]Krska R,Baumartner S,Josephs R.The state-of-the art in the analysis of type-A and-B trichithecend mycotoxins in cereals[J].Fres J Anal Chem,2001,371:285-299.
[11]Pestka JJ,Islam Z,Amuzie CJ.Immunochemical assessmentof deoxynivalenol tissue distribution following oralexposure in the mouse[J].Toxicol Lett,2008,178:83-87.
[12]食品安全监督抽检和风险监测工作规范[Z].Food safety supervision sampling inspection and risk monitoring work specifications[Z].
[13]食品安全监督抽检和风险监测实施细则[Z].Detailed rules for the implementation of food safety supervision,sampling inspection and risk monitoring[Z].
[14]GB 5009.209-2016食品安全国家标准食品中玉米赤霉烯酮的测定[S].GB 5009.209-2016 National food safety standard-Determination of zearalenone in food[S].
[15]GB 5009.111-2016食品安全国家标准食品中脱氧雪腐镰刀菌烯醇及其乙酰化衍生物的测定[S].GB 5009.111-2016 National food safety standard-Determination of deoxynivalenol and its acetylated derivatives in food[S].
[16]GB/T 27404-2008实验室质量控制规范食品理化检测[S].GB/T 27404-2008 Criterion on quality control of laboratories-Chemical testing of food[S].
[17]GB 2761-2017食品安全国家标准食品中真菌毒素限量[S].GB 2761-2017 National food safety standard-Limit of zearalenone mycotoxins in food[S].
[18]庄巧云,谢卫忠,方晓斌.关于小麦粉呕吐毒素(DON)的研究[J].现代农业,2017,2(10):78-80.Zhuang QY,Xie WZ,Fang XB.Study on wheat flour toxin(DON)[J].JMod Food,2017,2(10):78-80.
[2]Mishra HN,Chitrangada D.A review on biological control and metabolism of aflatoxin[J].Crit Rev Food Sci Nutr,2003,43:245-264.
[3]龚阿琼,罗金玲,胡骏鹏.2014年我国饲料原料中霉菌毒素含量的测定与分析[J].中国饲料,2015,(7):40-41.Gong AQ,Long JL,Hu JP.Detection and analysis of mycotoxin contamination of feed stuff in china in 2014[J].J Chin Feed,2015,(7):40-41.
[4]计成.霉菌毒素对家禽的危害及降解技术[J].中国家禽,2014,36(2):40-42.Ji C.The harm of mycotoxin to poultry and degradation technology[J].JChin Poul,2014,36(2):40-42.
[5]Mohamed EZ.Impact of mycotoxins on humans and animals[J].J Saud Chem Soc,2011,(15):129-144.
[6]王怡净,张立实.玉米赤霉烯酮毒性研究进展[J].中国食品卫生杂志.2002,14(5):41-43.Wang YJ,Zhang LS.Research progress of zearalenone toxicity[J].Chin JFood Hyg,2002,14(5):41-43.
[7]何庆华,许杨.玉米赤霉烯酮毒性研究及检测方法进展[J].卫生研究,2005,34(4):502-504.He QH,Xu Y.Advance in study on zearalenone’s toxicity and determination[J].J Hyg Res,2005,34(4):502-504.
[8]苗丽.常用饲料原料中玉米赤霉烯酮和呕吐毒素含量研究[D].泰安:山东农业大学,2015.Miao L.A field investigation of zearalenone and deoxynivalenol pollution in the common used feedstuffs[D].Taian:Shandong Agricultural University,2015.
[9]John CL,Josephine H,Irene P,et al.Workshopon Trichothecenes with a focus On DON:Sum-mary report[J].Toxicol Lett,2004,153:1-22.
[10]Krska R,Baumartner S,Josephs R.The state-of-the art in the analysis of type-A and-B trichithecend mycotoxins in cereals[J].Fres J Anal Chem,2001,371:285-299.
[11]Pestka JJ,Islam Z,Amuzie CJ.Immunochemical assessmentof deoxynivalenol tissue distribution following oralexposure in the mouse[J].Toxicol Lett,2008,178:83-87.
[12]食品安全监督抽检和风险监测工作规范[Z].Food safety supervision sampling inspection and risk monitoring work specifications[Z].
[13]食品安全监督抽检和风险监测实施细则[Z].Detailed rules for the implementation of food safety supervision,sampling inspection and risk monitoring[Z].
[14]GB 5009.209-2016食品安全国家标准食品中玉米赤霉烯酮的测定[S].GB 5009.209-2016 National food safety standard-Determination of zearalenone in food[S].
[15]GB 5009.111-2016食品安全国家标准食品中脱氧雪腐镰刀菌烯醇及其乙酰化衍生物的测定[S].GB 5009.111-2016 National food safety standard-Determination of deoxynivalenol and its acetylated derivatives in food[S].
[16]GB/T 27404-2008实验室质量控制规范食品理化检测[S].GB/T 27404-2008 Criterion on quality control of laboratories-Chemical testing of food[S].
[17]GB 2761-2017食品安全国家标准食品中真菌毒素限量[S].GB 2761-2017 National food safety standard-Limit of zearalenone mycotoxins in food[S].
[18]庄巧云,谢卫忠,方晓斌.关于小麦粉呕吐毒素(DON)的研究[J].现代农业,2017,2(10):78-80.Zhuang QY,Xie WZ,Fang XB.Study on wheat flour toxin(DON)[J].JMod Food,2017,2(10):78-80.