摘要
通过对钼铁中微量元素测定试验,应用盐酸等溶解酸溶样,优化了等离子体原子发射光谱分析的测定参数,并选择了元素的分析谱线,对钼铁中微量元素进行了准确测定。实验结果表明,各元素分析谱线线性相关性R>0.999 0,回收率在98%~105%。
In order to meet the needs of modern and rapid production,the determination of trace elements in ferromolybdenum was carried out in this paper,the dissolved acid sample such as hydrochloric acid was used to dissolve the sample.The determination parameters of plasma atomic emission spectrometry are optimized and the analytical spectrum line of elements was selected.The trace elements in ferromolybdenum were determined accurately.The experimental results showed that the linear correlation of the spectral lines of each element analysis was more than 0.999,and the recovery was between 98% and 105%.
引文
[1]邵常丽,王健君.ICP-AES法测定锰铁中微量硅[J].莱钢科技,2016(1):76.
[2]赵艳兵,刘爱坤,张瑞霖.ICP-AES法测定锰铁中微量铅[J].太钢科技,2010(2):94.