Modified disordered carbon prepared from 3,4,9,10-perylenetetracarboxylic dianhydride as an anode material for Li-ion batteries

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• 作者：Fei-biao Chen (1)
  Bo-rong Wu (1)
  Yun-kui Xiong (2)
  Wei-lin Liao (2)
  Dao-Bin Mu (1)
  Feng Wu (1)
  
  1. Beijing Key Laboratory of Environmental Science and Engineering ; School of Chemical Engineering and Environment ; Beijing Institute of Technology ; Beijing ; 100081 ; China
  2. Jiangxi Fine Chemical Key Laboratory ; Jiangxi Normal University ; Jiangxi ; 330027 ; China
  
• 关键词：carbon ; perylenetetracarboxylic dianhydride ; anode materials ; lithium ; ion batteries
• 刊名：International Journal of Minerals, Metallurgy, and Materials
• 出版年：2015
• 出版时间：February 2015
• 年：2015
• 卷：22
• 期：2
• 页码：203-209
• 全文大小：1,002 KB
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• 刊物类别：Chemistry and Materials Science
• 刊物主题：Materials Science
  Metallic Materials
  Mineral Resources
  
• 出版者：Journal Publishing Center of University of Science and Technology Beijing, in co-publication with Sp
• ISSN：1869-103X

文摘

To prepare an anode material for Li-ion batteries with high discharge capacity and good cycling stability, disordered carbon (DC) formed by calcinations of 3,4,9,10-perylenetetracarboxylic dianhydride was modified via an acid treatment using a mixture of HNO3 and H2SO4. The modified disordered carbon (MDC) was characterized by Fourier-transform infrared (FTIR) spectroscopy, X-ray diffraction (XRD) analysis, Brunauer-Emmett-Teller (BET) analysis, and scanning electron microscopy (SEM). FTIR spectra confirm the successful introduction of carbonyl groups onto the DC surface. Some pores appear in the columnar structure of MDC, as observed in SEM micrographs. Li+ ions intercalation/deintercalation is facilitated by the modified morphology. Electrochemical tests show that the MDC exhibits a significant improvement in discharge capacity and cycling stability. These results indicate that the MDC has strong potential for use as an anode material in Li-ion batteries.