- 中文主题词：钴 ; 化学分析和试验 ; 镍 ; 合金
- 标准号：ASTM E1473-2003
- 发布日期：2003
- 英文题名：Standard Test Methods for Chemical Analysis of Nickel, Cobalt, and High-Temperature Alloys
- 英文主题词：atomic ; absorption ; chemical analysis ; gravimetric ; ion exchange ; photometric ; titration
- 标准状态：现行
- 发布单位：US-ASTM
- 载体形态：38P.;A4
- 中国标准分类号：H13
- 国别：美国材料与试验协会
These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for compliance with compositional specifications, particularly those under the jurisdiction of ASTM Committee B-2 on Nonferrous Metals and Alloys. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E 882
1.1 These test methods describe the chemical analysis of nickel, cobalt, and high-temperature alloys having chemical compositions within the following limits:
| Element | Concentration Range, % |
| Aluminum | 0.005 to 7.00 |
| Beryllium | 0.001 to 0.05 |
| Boron | 0.001 to 1.00 |
| Calcium | 0.002 to 0.05 |
| Carbon | 0.001 to 1.10 |
| Chromium | 0.10 to 33.00 |
| Cobalt | 0.10 to 75.00 |
| Copper | 0.01 to 35.00 |
| Iron | 0.01 to 50.00 |
| Lead | 0.001 to 0.01 |
| Magnesium | 0.001 to 0.05 |
| Manganese | 0.01 to 3.0 |
| Molybdenum | 0.01 to 30.0 |
| Niobium (Columbium) | 0.01 to 6.0 |
| Nickel | 0.10 to 98.0 |
| Nitrogen | 0.001 to 0.20 |
| Phosphorus | 0.002 to 0.08 |
| Sulfur | 0.002 to 0.10 |
| Silicon | 0.01 to 5.00 |
| Tantalum | 0.005 to 1.00 |
| Tin | 0.002 to 0.10 |
| Titanium | 0.01 to 5.00 |
| Tungsten | 0.01 to 18.00 |
| Vanadium | 0.01 to 3.25 |
| Zinc | 0.001 to 0.01 |
| Zirconium | 0.01 to 2.50 |
1.2 The test methods in this standard are contained in the sections indicated as follows:
| Sections | |
| Aluminum, Total by the 8-Quinolinol Gravimetric Method (0.20 to7.00 %) | 62 to 69 |
| Chromium by the Atomic Absorption Method (0.018 to 1.00 %) | 100 to 109 |
| Chromium by the Peroxydisulfate Oxidation-Titration Method(0.10 to 33.00 %) | 110 to 118 |
| Cobalt by the Ion-Exchange-Potentiometric Titration Method (2 to75 %) | 34 to 41 |
| Cobalt by the Nitroso-R-Salt Photometric Method (0.10 to5.0 %) | 42 to 51 |
| Copper by Neocuproine Photometric Method (0.010 to 10.00 %) | 52 to 61 |
| Iron by the Silver Reduction Titrimetric Method (1.0 to 50.0 %) | 127 to 134 |
| Manganese by the Metaperiodate Photometric Method (0.05 to2.00 %) | 8 to 17 |
| Molybdenum by the Ion Exchange-8-Hydroxyquinoline Gravi-metric Method (1.5 to 30 %) | 119 to 126 |
| Molybdenum by the Photometric Method (0.01 to 1.50 %) | 88 to 99 |
| Nickel by the Dimethylglyoxime Gravimetric Method (0.1 to84.0 %) | 70 to 77 |
| Niobium by the Ion Exchange-Cupferron Gravimetric Method(0.5 to 6.0 %) | 135 to 142 |
| Silicon by the Gravimetric Method (0.05 to 5.00 %) | 27 to 33 |
| Sulfur by the Combustion-Iodate Titration Method (0.006 to0.1 %) | 18 to 26 |
| Tantalum by the Ion Exchange-Pyrogallol SpectrophotometricMethod (0.03 to 1.0%) | 143 to 151 |
| Tin by the Solvent Extraction-Atomic Absorption Method (0.002to 0.10 %) | 78 to 87 |
1.3 Methods for the determination of several elements not included in these t......
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